[4-2H]-3-dehydroshikimic acid

Base Information

Chemical Name:[4-2H]-3-dehydroshikimic acid
CAS No.:323195-33-1
Molecular Formula:C₇H₈O₅
Molecular Weight:173.13
Hs Code.:

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Chemical Property of [4-2H]-3-dehydroshikimic acid

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Technology Process of [4-2H]-3-dehydroshikimic acid

There total 2 articles about [4-2H]-3-dehydroshikimic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32470-29-4
[2,2,4-2H₃]-3-dehydroquinic acid

: 323195-33-1
[4-2H]-3-dehydroshikimic acid

Guidance literature:: With A_. nidulans dehydroquinase type II; E_. coli dehydroquinase type I; In water; at 20 ℃; for 122h;
DOI:10.1006/bioo.2000.1174

Reference yield:

: 10534-44-8
3-dehydroquinic acid

: 323195-33-1
[4-2H]-3-dehydroshikimic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(dimethylamino)pyridine; D₂O / 168 h / 20 °C / pH 9.5

2: E_. coli dehydroquinase type I; A_. nidulans dehydroquinase type II / H₂O / 122 h / 20 °C

With dmap; A_. nidulans dehydroquinase type II; E_. coli dehydroquinase type I; water-d2; In water;
DOI:10.1006/bioo.2000.1174

Reference yield:

: 323195-33-1
[4-2H]-3-dehydroshikimic acid

: C₁₀H₈⁽²⁾HO₁₀P^(4-)*4K⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: 9 mg / triethanolamine; NADPH; shikimate dehydrogenase / 24 h / 20 °C / pH 6.5

2.1: EPSP synthase; Escherichia coli shikimate kinase; ATP K+ salt / MgCl₂ / various solvent(s) / 24 h / 30 °C / pH 7.5

2.2: apyrase (Sigma grade VII); NaCl / 30 °C

With triethanolamine; ATP K+ salt; EPSP synthase; Escherichia coli shikimate kinase; shikimate dehydrogenase; NADPH; magnesium chloride; In various solvent(s);
DOI:10.1006/bioo.2000.1174