3-chloro-3-methyl-2-nitroso-5-phenylpentanol

Base Information

Chemical Name:3-chloro-3-methyl-2-nitroso-5-phenylpentanol
CAS No.:101210-90-6
Molecular Formula:C₂₄H₃₂Cl₂N₂O₄
Molecular Weight:483.435
Hs Code.:

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Chemical Property of 3-chloro-3-methyl-2-nitroso-5-phenylpentanol

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Technology Process of 3-chloro-3-methyl-2-nitroso-5-phenylpentanol

There total 3 articles about 3-chloro-3-methyl-2-nitroso-5-phenylpentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 55066-44-9
3-methyl-5-phenylpent-2-en-1-ol

: 101210-90-6
3-chloro-3-methyl-2-nitroso-5-phenylpentanol

Guidance literature:: With hydrogenchloride; 1-methylbutyl nitrite; In acetic acid; 0 deg C, -78 deg C, 10 min, 0 deg C,;

Reference yield:

: 2550-26-7
4-Phenyl-2-butanone

: 101210-90-6
3-chloro-3-methyl-2-nitroso-5-phenylpentanol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / sodium hydride / toluene / 1.) 0.5 h, r.t., 2.) 70 deg C, 2 h,

2: 80 percent / lithium aluminium hydride / diethyl ether / 0 deg C, 8 deg C, r.t. overnight

3: 26 percent / conc. hydrochloric acid, 2-pentyl nitrite / acetic acid / 0 deg C, -78 deg C, 10 min, 0 deg C,

With hydrogenchloride; lithium aluminium tetrahydride; 1-methylbutyl nitrite; sodium hydride; In diethyl ether; acetic acid; toluene;

Reference yield:

: ethyl 3-methyl-5-phenylpent-2-enoate

: 101210-90-6
3-chloro-3-methyl-2-nitroso-5-phenylpentanol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / lithium aluminium hydride / diethyl ether / 0 deg C, 8 deg C, r.t. overnight

2: 26 percent / conc. hydrochloric acid, 2-pentyl nitrite / acetic acid / 0 deg C, -78 deg C, 10 min, 0 deg C,

With hydrogenchloride; lithium aluminium tetrahydride; 1-methylbutyl nitrite; In diethyl ether; acetic acid;