Technology Process of C13H16O5
There total 5 articles about C13H16O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
chromium(VI) oxide; sulfuric acid;
In
water; acetone;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1002/chem.201003591
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol; water / 0.5 h / 20 °C / Inert atmosphere
2: chromium(VI) oxide; sulfuric acid / water; acetone / 2 h / 20 °C / Inert atmosphere
With
chromium(VI) oxide; sodium tetrahydroborate; nickel(II) chloride hexahydrate; sulfuric acid;
In
methanol; water; acetone;
DOI:10.1002/chem.201003591
- Guidance literature:
-
Multi-step reaction with 4 steps
1: silver(l) oxide / diethyl ether / 20 °C / Inert atmosphere; Reflux; Darkness
2: Hoveyda-Grubbs catalyst second generation / dichloromethane / 20 °C / Inert atmosphere
3: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol; water / 0.5 h / 20 °C / Inert atmosphere
4: chromium(VI) oxide; sulfuric acid / water; acetone / 2 h / 20 °C / Inert atmosphere
With
chromium(VI) oxide; sodium tetrahydroborate; Hoveyda-Grubbs catalyst second generation; nickel(II) chloride hexahydrate; sulfuric acid; silver(l) oxide;
In
methanol; diethyl ether; dichloromethane; water; acetone;
DOI:10.1002/chem.201003591