ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolidineheptanoate

Base Information

Chemical Name:ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolidineheptanoate
CAS No.:136494-28-5
Molecular Formula:C₂₈H₄₄N₂O₄
Molecular Weight:472.668
Hs Code.:

Synonyms:

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Chemical Property of ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolidineheptanoate

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Technology Process of ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolidineheptanoate

There total 10 articles about ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolidineheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65706-29-8
diethyl 2-(3-cyclohexyl-3-hydroxypropyl)aminononanedioate

: 136494-28-5,136494-29-6
ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolidineheptanoate

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 2 h / Ambient temperature

2: 1,8-diazabicyclo<5.4.0>undec-7-ene / toluene / 1.) room temp., 16 h 2.) 60 deg C, 1 h

3: 56 percent / NaBH₄, acetic acid / propan-2-ol / 1.) 3 h 2.) room temp., overnight

4: 1.) triethylsilane, trifluoroacetic acid 2.) water, K₂CO₃ / 1.) 50 deg C 2.) methanol, room temp.

With triethylsilane; sodium tetrahydroborate; water; potassium carbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In isopropyl alcohol; toluene;
DOI:10.1002/ardp.2503240802

Reference yield:

: 65706-29-8
diethyl 2-(3-cyclohexyl-3-hydroxypropyl)aminononanedioate

: 136494-28-5,136494-29-6
ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolidineheptanoate

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 2 h / Ambient temperature

2: 1,8-diazabicyclo<5.4.0>undec-7-ene / toluene / 1.) room temp., 16 h 2.) 60 deg C, 1 h

3: 56 percent / NaBH₄, acetic acid / propan-2-ol / 1.) 3 h 2.) room temp., overnight

4: 1.) triethylsilane, trifluoroacetic acid 2.) water, K₂CO₃ / 1.) 50 deg C 2.) methanol, room temp.

With triethylsilane; sodium tetrahydroborate; water; potassium carbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In isopropyl alcohol; toluene;
DOI:10.1002/ardp.2503240802

Reference yield:

: 136494-22-9,136494-23-0
ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2,5-dioxo-4-imidazolidineheptanoate

: 136494-28-5,136494-29-6
ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolidineheptanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / NaBH₄, acetic acid / propan-2-ol / 1.) 3 h 2.) room temp., overnight

2: 1.) triethylsilane, trifluoroacetic acid 2.) water, K₂CO₃ / 1.) 50 deg C 2.) methanol, room temp.

With triethylsilane; sodium tetrahydroborate; water; potassium carbonate; acetic acid; trifluoroacetic acid; In isopropyl alcohol;
DOI:10.1002/ardp.2503240802