(3S)-2,3-diacetoxy-N-benzyloxycarbonylpiperidine

Base Information

Chemical Name:(3S)-2,3-diacetoxy-N-benzyloxycarbonylpiperidine
CAS No.:330798-22-6
Molecular Formula:C₁₇H₂₁NO₆
Molecular Weight:335.357
Hs Code.:

Synonyms:

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Chemical Property of (3S)-2,3-diacetoxy-N-benzyloxycarbonylpiperidine

Chemical Property:

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Technology Process of (3S)-2,3-diacetoxy-N-benzyloxycarbonylpiperidine

There total 8 articles about (3S)-2,3-diacetoxy-N-benzyloxycarbonylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-5-Azido-2-hydroxy-pentanoic acid methoxy-methyl-amide

: 330798-22-6
(3S)-2,3-diacetoxy-N-benzyloxycarbonylpiperidine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂; aq.HCl / Pd/C / ethanol / 3 h / 7600.51 Torr

2: NaHCO₃ / tetrahydrofuran; H₂O / 1 h / 0 °C

3: 91 percent / LiAlH₄ / diethyl ether / 1.5 h / 0 °C

4: triethylamine / 4-N,N-dimethylaminopyridine / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium hydrogencarbonate; triethylamine; dmap; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; water;
DOI:10.1021/jo001297m

Reference yield:

: (S)-5-Amino-2-hydroxy-pentanoic acid methoxy-methyl-amide

: 330798-22-6
(3S)-2,3-diacetoxy-N-benzyloxycarbonylpiperidine

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃ / tetrahydrofuran; H₂O / 1 h / 0 °C

2: 91 percent / LiAlH₄ / diethyl ether / 1.5 h / 0 °C

3: triethylamine / 4-N,N-dimethylaminopyridine / 20 °C

With lithium aluminium tetrahydride; sodium hydrogencarbonate; triethylamine; dmap; In tetrahydrofuran; diethyl ether; water;
DOI:10.1021/jo001297m

Reference yield:

: 2-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-pentanoic acid methoxy-methyl-amide

: 330798-22-6
(3S)-2,3-diacetoxy-N-benzyloxycarbonylpiperidine

Guidance literature:: Multi-step reaction with 6 steps

1: aq. HCl / tetrahydrofuran / 5 h / 20 °C

2: triphenylphosphine; diphenylphosphoryl azide; DEAD / tetrahydrofuran / 1 h / 20 °C

3: H₂; aq.HCl / Pd/C / ethanol / 3 h / 7600.51 Torr

4: NaHCO₃ / tetrahydrofuran; H₂O / 1 h / 0 °C

5: 91 percent / LiAlH₄ / diethyl ether / 1.5 h / 0 °C

6: triethylamine / 4-N,N-dimethylaminopyridine / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; diphenylphosphoranyl azide; hydrogen; sodium hydrogencarbonate; triethylamine; triphenylphosphine; diethylazodicarboxylate; dmap; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; water; 2: Mitsunobu reaction;
DOI:10.1021/jo001297m