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C28H32NO8P

Base Information
  • Chemical Name:C28H32NO8P
  • CAS No.:1450984-48-1
  • Molecular Formula:C28H32NO8P
  • Molecular Weight:541.538
  • Hs Code.:
C<sub>28</sub>H<sub>32</sub>NO<sub>8</sub>P

Synonyms:

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Chemical Property of C28H32NO8P
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Technology Process of C28H32NO8P

There total 15 articles about C28H32NO8P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c3md00033h
Guidance literature:
Multi-step reaction with 14 steps
1: 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1.5 h / 0 - 25 °C / Inert atmosphere
2: boron trifluoride diethyl etherate / acetone / 15 h / 25 °C / Inert atmosphere
3: diethyl ether / 2 h / -78 °C / Inert atmosphere
4: zinc tetrahydridoborate*Et2O; cerium(III) chloride heptahydrate / methanol / 2.5 h / 0 - 25 °C / Inert atmosphere
5: water; acetic acid / 15 h / 50 °C
6: pyridine / 1 h / 0 °C / Inert atmosphere
7: pyridine / 0.67 h / 0 - 25 °C / Inert atmosphere
8: acetonitrile / 1.5 h / 0 - 25 °C / Inert atmosphere
9: sodium chloride / ethyl acetate; water; acetonitrile / 0.5 h / 25 °C
10: sodium tetrahydroborate; oxygen / N,N-dimethyl-formamide / 3 h / 25 °C
11: 1H-tetrazole / dichloromethane / 2 h / 0 - 25 °C / Inert atmosphere
12: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / Inert atmosphere
13: sodium methylate; methanol / dichloromethane / 0.5 h / 25 °C / Inert atmosphere
14: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 25 °C / Inert atmosphere
With 4-methyl-morpholine; pyridine; 1H-tetrazole; methanol; sodium tetrahydroborate; zinc tetrahydridoborate*Et2O; cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; oxygen; sodium methylate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; sodium chloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1039/c3md00033h
Guidance literature:
Multi-step reaction with 12 steps
1: diethyl ether / 2 h / -78 °C / Inert atmosphere
2: zinc tetrahydridoborate*Et2O; cerium(III) chloride heptahydrate / methanol / 2.5 h / 0 - 25 °C / Inert atmosphere
3: water; acetic acid / 15 h / 50 °C
4: pyridine / 1 h / 0 °C / Inert atmosphere
5: pyridine / 0.67 h / 0 - 25 °C / Inert atmosphere
6: acetonitrile / 1.5 h / 0 - 25 °C / Inert atmosphere
7: sodium chloride / ethyl acetate; water; acetonitrile / 0.5 h / 25 °C
8: sodium tetrahydroborate; oxygen / N,N-dimethyl-formamide / 3 h / 25 °C
9: 1H-tetrazole / dichloromethane / 2 h / 0 - 25 °C / Inert atmosphere
10: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / Inert atmosphere
11: sodium methylate; methanol / dichloromethane / 0.5 h / 25 °C / Inert atmosphere
12: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 25 °C / Inert atmosphere
With pyridine; 1H-tetrazole; methanol; sodium tetrahydroborate; zinc tetrahydridoborate*Et2O; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; water; oxygen; sodium methylate; acetic acid; 3-chloro-benzenecarboperoxoic acid; sodium chloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3md00033h
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