C₅₀H₄₁F₇N₄O₁₉

Base Information

Chemical Name:C₅₀H₄₁F₇N₄O₁₉
CAS No.:118173-22-1
Molecular Formula:C₅₀H₄₁F₇N₄O₁₉
Molecular Weight:1134.88
Hs Code.:

C<sub>50</sub>H<sub>41</sub>F<sub>7</sub>N<sub>4</sub>O<sub>19</sub>

Synonyms:

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Chemical Property of C₅₀H₄₁F₇N₄O₁₉

Chemical Property:

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Technology Process of C₅₀H₄₁F₇N₄O₁₉

There total 6 articles about C₅₀H₄₁F₇N₄O₁₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65399-05-5
5-amino-3H-isobenzofuran-1-one

: 118173-22-1
C₅₀H₄₁F₇N₄O₁₉

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) 40 percent aq. HPF₆, 2.) NaNO₂ / 1.) water, 0 deg C, 2.) water

2: 1,3,5-trimethyl-benzene / Heating

4: 1.) i-Pr₂NH, n-BuLi / 1.) THF, 2.) THF

5: 98 percent / BCl₃ / CH₂Cl₂ / 0.5 h / -78 °C

6: 1.) TMS-triflate, 4 Angstroem molecular sieve / 1.) CH₂Cl₂, ether, -42 deg C, then 0 deg C, 1 h, 2.) CH₂Cl₂, then -30 deg C, overnight

With hexafluorophosphoric acid; n-butyllithium; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; boron trichloride; diisopropylamine; sodium nitrite; In dichloromethane; 1,3,5-trimethyl-benzene;
DOI:10.1016/S0040-4020(01)86162-7

Reference yield:

: 700-85-6
5-fluoroisobenzofuran-1(3H)-one

: 118173-22-1
C₅₀H₄₁F₇N₄O₁₉

Guidance literature:: Multi-step reaction with 4 steps

2: 1.) i-Pr₂NH, n-BuLi / 1.) THF, 2.) THF

3: 98 percent / BCl₃ / CH₂Cl₂ / 0.5 h / -78 °C

4: 1.) TMS-triflate, 4 Angstroem molecular sieve / 1.) CH₂Cl₂, ether, -42 deg C, then 0 deg C, 1 h, 2.) CH₂Cl₂, then -30 deg C, overnight

With n-butyllithium; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; boron trichloride; diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4020(01)86162-7

Reference yield:

: 105398-60-5
5-fluoro-3-oxo-1,3-dihydroisobenzofuran-1-carbonitrile

: 118173-22-1
C₅₀H₄₁F₇N₄O₁₉

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) i-Pr₂NH, n-BuLi / 1.) THF, 2.) THF

2: 98 percent / BCl₃ / CH₂Cl₂ / 0.5 h / -78 °C

3: 1.) TMS-triflate, 4 Angstroem molecular sieve / 1.) CH₂Cl₂, ether, -42 deg C, then 0 deg C, 1 h, 2.) CH₂Cl₂, then -30 deg C, overnight

With n-butyllithium; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; boron trichloride; diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4020(01)86162-7