(3S,5S,6S,3'S,4'R)-(+)-4-(tert-butoxycarbonyl)-6-[1'-(tert-butyldiphenylsiloxy)-3',4'-O-isopropylidenehexane-6'-yl]-5-ethyloxycarbonyl-3-metyl-2-piperazinone

Base Information

• Chemical Name: (3S,5S,6S,3'S,4'R)-(+)-4-(tert-butoxycarbonyl)-6-[1'-(tert-butyldiphenylsiloxy)-3',4'-O-isopropylidenehexane-6'-yl]-5-ethyloxycarbonyl-3-metyl-2-piperazinone
• CAS No.: 1089174-22-0
• Molecular Formula: C₃₈H₅₆N₂O₈Si
• Molecular Weight: 696.957
• Mol file: 1089174-22-0.mol

Synonyms:

Chemical Property of (3S,5S,6S,3'S,4'R)-(+)-4-(tert-butoxycarbonyl)-6-[1'-(tert-butyldiphenylsiloxy)-3',4'-O-isopropylidenehexane-6'-yl]-5-ethyloxycarbonyl-3-metyl-2-piperazinone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3S,5S,6S,3'S,4'R)-(+)-4-(tert-butoxycarbonyl)-6-[1'-(tert-butyldiphenylsiloxy)-3',4'-O-isopropylidenehexane-6'-yl]-5-ethyloxycarbonyl-3-metyl-2-piperazinone

There total 1 articles about (3S,5S,6S,3'S,4'R)-(+)-4-(tert-butoxycarbonyl)-6-[1'-(tert-butyldiphenylsiloxy)-3',4'-O-isopropylidenehexane-6'-yl]-5-ethyloxycarbonyl-3-metyl-2-piperazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + C33H48N2O6Si → (3S,5S,6S,3'S,4'R)-(+)-4-(tert-butoxycarbonyl)-6-[1'-(tert-butyldiphenylsiloxy)-3',4'-O-isopropylidenehexane-6'-yl]-5-ethyloxycarbonyl-3-metyl-2-piperazinone (1089174-22-0)

Guidance literature:

In ethyl acetate; at 20 - 80 ℃; Inert atmosphere;

DOI:10.1002/chem.200801024

Reference yield:

(3S,5S,6S,3'S,4'R)-(+)-4-(tert-butoxycarbonyl)-6-[1'-(tert-butyldiphenylsiloxy)-3',4'-O-isopropylidenehexane-6'-yl]-5-ethyloxycarbonyl-3-metyl-2-piperazinone (1089174-22-0) → C36H52N2O8Si

Guidance literature:

With lithium hydroxide; water; In tetrahydrofuran; methanol; at 20 ℃;

DOI:10.1002/chem.200801024

upstream raw materials:

di-tert-butyl dicarbonate