Technology Process of C20H30O6S
There total 3 articles about C20H30O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
chloroform-d1;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ja211840k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: porcine pancreatic lipase Sigma type 2 / 1 h / Molecular sieve; Inert atmosphere; Enzymatic reaction
1.2: 120 h / 20 °C / Inert atmosphere; Enzymatic reaction
2.1: potassium dihydrogenphosphate; porcine pancreatic lipase Sigma type 2; sodium hydroxide / water / 23 h / 20 °C / Inert atmosphere; Enzymatic reaction
3.1: triethylamine / chloroform-d1 / 20 °C / Inert atmosphere
With
potassium dihydrogenphosphate; porcine pancreatic lipase Sigma type 2; triethylamine; sodium hydroxide;
In
chloroform-d1; water;
DOI:10.1021/ja211840k
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 4.17 h / 0 °C / Inert atmosphere
2.1: porcine pancreatic lipase Sigma type 2 / 1 h / Molecular sieve; Inert atmosphere; Enzymatic reaction
2.2: 120 h / 20 °C / Inert atmosphere; Enzymatic reaction
3.1: potassium dihydrogenphosphate; porcine pancreatic lipase Sigma type 2; sodium hydroxide / water / 23 h / 20 °C / Inert atmosphere; Enzymatic reaction
4.1: triethylamine / chloroform-d1 / 20 °C / Inert atmosphere
With
potassium dihydrogenphosphate; lithium aluminium tetrahydride; porcine pancreatic lipase Sigma type 2; triethylamine; sodium hydroxide;
In
tetrahydrofuran; chloroform-d1; water;
DOI:10.1021/ja211840k
