Technology Process of C44H10F20N4
There total 4 articles about C44H10F20N4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C44H18F20N4O;
With
boron trifluoride diethyl etherate;
Inert atmosphere;
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
Inert atmosphere;
DOI:10.1002/chem.201103034
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / Inert atmosphere
2.1: boron trifluoride diethyl etherate / Inert atmosphere
2.2: Inert atmosphere
With
sodium tetrahydroborate; boron trifluoride diethyl etherate;
In
tetrahydrofuran; methanol;
DOI:10.1002/chem.201103034
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.08 h / 20 °C / Inert atmosphere
3.1: ethylmagnesium bromide / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere
3.2: -78 - 0 °C / Inert atmosphere
4.1: sodium tetrahydroborate / tetrahydrofuran; methanol / Inert atmosphere
5.1: boron trifluoride diethyl etherate / Inert atmosphere
5.2: Inert atmosphere
With
sodium tetrahydroborate; boron trifluoride diethyl etherate; ethylmagnesium bromide; tetrabutyl ammonium fluoride; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/chem.201103034