C₂₅H₃₄O₅Si

Base Information

Chemical Name:C₂₅H₃₄O₅Si
CAS No.:1373334-12-3
Molecular Formula:C₂₅H₃₄O₅Si
Molecular Weight:442.627
Hs Code.:

C<sub>25</sub>H<sub>34</sub>O<sub>5</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₄O₅Si

Chemical Property:

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Technology Process of C₂₅H₃₄O₅Si

There total 9 articles about C₂₅H₃₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7759-23-1
O-acetylisophotosantonic lactone

: 1373334-12-3
C₂₅H₃₄O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: methanol; potassium carbonate / 20 °C

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h

3.1: sodium hydrogencarbonate / methanol / 25 h / 20 °C

4.1: 1H-imidazole / dichloromethane / 2 h / 20 °C

5.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.67 h / -78 °C

5.2: 0.5 h / -78 °C

6.1: palladium diacetate / acetonitrile / 12 h / 20 °C

7.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 0.5 h / 0 °C

8.1: dmap; N-ethyl-N,N-diisopropylamine

With 1H-imidazole; methanol; dmap; sodium tetrahydroborate; cerium(III) chloride heptahydrate; palladium 10% on activated carbon; hydrogen; palladium diacetate; potassium hexamethylsilazane; sodium hydrogencarbonate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; acetonitrile; 6.1: Saegusa oxidation;
DOI:10.5012/bkcs.2012.33.1.289

Reference yield:

: 1373334-11-2
C₁₈H₃₀O₄Si

: 1373334-12-3
C₂₅H₃₄O₅Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.67 h / -78 °C

1.2: 0.5 h / -78 °C

2.1: palladium diacetate / acetonitrile / 12 h / 20 °C

3.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 0.5 h / 0 °C

4.1: dmap; N-ethyl-N,N-diisopropylamine

With dmap; sodium tetrahydroborate; cerium(III) chloride heptahydrate; palladium diacetate; potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; toluene; acetonitrile; 2.1: Saegusa oxidation;
DOI:10.5012/bkcs.2012.33.1.289

Reference yield:

: C₂₁H₃₈O₄Si₂

: 1373334-12-3
C₂₅H₃₄O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate / acetonitrile / 12 h / 20 °C

2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 0.5 h / 0 °C

3: dmap; N-ethyl-N,N-diisopropylamine

With dmap; sodium tetrahydroborate; cerium(III) chloride heptahydrate; palladium diacetate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; acetonitrile; 1: Saegusa oxidation;
DOI:10.5012/bkcs.2012.33.1.289