C₁₄H₂₂N₂O₂

Base Information

• Chemical Name: C₁₄H₂₂N₂O₂
• CAS No.: 1390640-00-2
• Molecular Formula: C₁₄H₂₂N₂O₂
• Molecular Weight: 250.341
• Mol file: 1390640-00-2.mol

Synonyms:

Chemical Property of C₁₄H₂₂N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₂N₂O₂

There total 9 articles about C₁₄H₂₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H34N2O4 → C14H22N2O2 (1390640-00-2)

Guidance literature:

C₂₂H₃₄N₂O₄; With hydrogenchloride; In methanol; water; at 40 ℃; Inert atmosphere;

DOI:10.1039/c2ob25727k

Reference yield:

C15H21NO3 (1390639-87-8) → C14H22N2O2 (1390640-00-2)

Guidance literature:

Multi-step reaction with 9 steps

1.1: tetrahydrofuran / 7 h / 0 - 20 °C / Inert atmosphere

2.1: pyridine; methanesulfonyl chloride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

3.1: alpha AD-mix / water; acetone / 35 h / 0 - 4 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; ammonium formate / methanol / 1.5 h / 60 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

6.1: sodium periodate / ethanol; water / 1 h / 20 °C / Inert atmosphere

7.1: magnesium sulfate / dichloromethane / 5 h / 20 °C / Inert atmosphere

8.1: sodium tetrahydroborate / methanol / 0 - 20 °C / Inert atmosphere

9.1: hydrogenchloride / methanol; water / 40 °C / Inert atmosphere

9.2: Amberlyst_.(R). A-26 (OH-)

With pyridine; hydrogenchloride; sodium tetrahydroborate; sodium periodate; palladium 10% on activated carbon; alpha AD-mix; ammonium formate; magnesium sulfate; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetone;

DOI:10.1039/c2ob25727k

Reference yield:

C18H27NO4 (1390639-92-5) → C14H22N2O2 (1390640-00-2)

Guidance literature:

Multi-step reaction with 6 steps

1.1: palladium 10% on activated carbon; ammonium formate / methanol / 1.5 h / 60 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

3.1: sodium periodate / ethanol; water / 1 h / 20 °C / Inert atmosphere

4.1: magnesium sulfate / dichloromethane / 5 h / 20 °C / Inert atmosphere

5.1: sodium tetrahydroborate / methanol / 0 - 20 °C / Inert atmosphere

6.1: hydrogenchloride / methanol; water / 40 °C / Inert atmosphere

6.2: Amberlyst_.(R). A-26 (OH-)

With hydrogenchloride; sodium tetrahydroborate; sodium periodate; palladium 10% on activated carbon; ammonium formate; magnesium sulfate; triethylamine; In methanol; ethanol; dichloromethane; water;

DOI:10.1039/c2ob25727k

upstream raw materials:

C₁₅H₂₁NO₃

C₁₈H₂₇NO₃

C₁₈H₂₅NO₂

C₁₈H₂₇NO₄