Pentadecanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Base Information

Chemical Name:Pentadecanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide
CAS No.:848827-51-0
Molecular Formula:C₅₉H₉₀N₂O₈
Molecular Weight:955.372
Hs Code.:

Pentadecanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

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Chemical Property of Pentadecanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

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Technology Process of Pentadecanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

There total 4 articles about Pentadecanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-3-Hydroxy-2-pentadecanoylamino-propionic acid methyl ester

: 848827-51-0
Pentadecanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodosuccinimide; molecular sieves 4 Angstroem; trifluoromethanesulfonic acid / CH₂Cl₂ / -15 - -10 °C

2: sodium hydroxide / H₂O; tetrahydrofuran

3: 1-hydroxybenzotriazole hydrate / 1,2-dichloro-ethane; CH₂Cl₂

With sodium hydroxide; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; 1-hydroxybenzotriazol-hydrate; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2004.12.027

Reference yield:

: 848827-49-6
(S)-3-((2R,4aR,6S,7R,8S,8aR)-7,8-Bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-2-pentadecanoylamino-propionic acid methyl ester

: 848827-51-0
Pentadecanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / H₂O; tetrahydrofuran

2: 1-hydroxybenzotriazole hydrate / 1,2-dichloro-ethane; CH₂Cl₂

With sodium hydroxide; 1-hydroxybenzotriazol-hydrate; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2004.12.027

Reference yield:

: 87470-70-0
S-phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-thio-β-D-glucopyranoside

: 848827-51-0
Pentadecanoic acid [(S)-2-((2R,4aR,6S,7R,8S,8aR)-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-1-tetradecylcarbamoyl-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodosuccinimide; molecular sieves 4 Angstroem; trifluoromethanesulfonic acid / CH₂Cl₂ / -15 - -10 °C

2: sodium hydroxide / H₂O; tetrahydrofuran

3: 1-hydroxybenzotriazole hydrate / 1,2-dichloro-ethane; CH₂Cl₂

With sodium hydroxide; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; 1-hydroxybenzotriazol-hydrate; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2004.12.027