4-Chlorobenzaldehyde N-phenylthiosemicarbazone

Base Information

Chemical Name:4-Chlorobenzaldehyde N-phenylthiosemicarbazone
CAS No.:74959-65-2
Molecular Formula:C14H12 Cl N3 S
Molecular Weight:289.788
Hs Code.:
European Community (EC) Number:656-475-5
NSC Number:231522
DSSTox Substance ID:DTXSID00430626
ChEMBL ID:CHEMBL251896

Synonyms:NSC231522;74959-65-2;CHEMBL251896;DTXSID00430626;SALOR-INT L453382-1EA;AKOS002201746;NSC-231522;4-chlorobenzaldehyde 4-phenyl-3-thiosemicarbazone;3-[(E)-(4-Chlorobenzylidene)amino]-1-phenylthiourea;4-CHLOROBENZALDEHYDE N-PHENYLTHIOSEMICARBAZONE;1-[(E)-(4-chlorophenyl)methyleneamino]-3-phenyl-thiourea

Suppliers and Price of 4-Chlorobenzaldehyde N-phenylthiosemicarbazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 4-Chlorobenzaldehyde N-phenylthiosemicarbazone

Chemical Property:

Vapor Pressure:4.5E-07mmHg at 25°C
Boiling Point:414.3°C at 760 mmHg
Flash Point:204.3°C
Density:1.24g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:289.0440463
Heavy Atom Count:19
Complexity:308

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=S)NN=CC2=CC=C(C=C2)Cl
Isomeric SMILES:C1=CC=C(C=C1)NC(=S)N/N=C/C2=CC=C(C=C2)Cl

Technology Process of 4-Chlorobenzaldehyde N-phenylthiosemicarbazone

There total 3 articles about 4-Chlorobenzaldehyde N-phenylthiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 83639-14-9,34025-60-0
2,4-bis(4-chlorophenyl)-3-azabicyclo[3.3.1]nonan-9-one

: 5351-69-9
4-Phenyl-3-thiosemicarbazide

: C₂₇H₂₆Cl₂N₄S

: 74959-65-2
2-(4-chlorobenzylidene)-N-phenylhydrazinecarbothioamide

Guidance literature:: In ethanol; chloroform; at 90 - 100 ℃; for 96h; Acidic conditions;
DOI:10.3109/14756366.2010.525508

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 5351-69-9
4-Phenyl-3-thiosemicarbazide

: 74959-65-2
2-(4-chlorobenzylidene)-N-phenylhydrazinecarbothioamide

Guidance literature:: With hydrogenchloride; In ethanol; Heating;
DOI:10.1007/BF00809296

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 104-88-1
4-chlorobenzaldehyde

: C₂₇H₂₆Cl₂N₄S

: 74959-65-2
2-(4-chlorobenzylidene)-N-phenylhydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / ethanol / 20 °C

2: ethanol; chloroform / 96 h / 90 - 100 °C / Acidic conditions

With ammonium acetate; In ethanol; chloroform;
DOI:10.3109/14756366.2010.525508