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4-{(Z)-[(1S,3aS,7aS)-1-(isoquinolin-7-yl)-7a-methyltetrahydro-1H-inden-5(6H,7H,7aH)-ylidene]methyl}-N,N-dimethylcyclohex-3-enamine

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  • Chemical Name:4-{(Z)-[(1S,3aS,7aS)-1-(isoquinolin-7-yl)-7a-methyltetrahydro-1H-inden-5(6H,7H,7aH)-ylidene]methyl}-N,N-dimethylcyclohex-3-enamine
  • CAS No.:1388055-02-4
  • Molecular Formula:C28H36N2
  • Molecular Weight:400.607
  • Hs Code.:
  • Mol file:1388055-02-4.mol
4-{(Z)-[(1S,3aS,7aS)-1-(isoquinolin-7-yl)-7a-methyltetrahydro-1H-inden-5(6H,7H,7aH)-ylidene]methyl}-N,N-dimethylcyclohex-3-enamine

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Chemical Property of 4-{(Z)-[(1S,3aS,7aS)-1-(isoquinolin-7-yl)-7a-methyltetrahydro-1H-inden-5(6H,7H,7aH)-ylidene]methyl}-N,N-dimethylcyclohex-3-enamine Edit
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Technology Process of 4-{(Z)-[(1S,3aS,7aS)-1-(isoquinolin-7-yl)-7a-methyltetrahydro-1H-inden-5(6H,7H,7aH)-ylidene]methyl}-N,N-dimethylcyclohex-3-enamine

There total 12 articles about 4-{(Z)-[(1S,3aS,7aS)-1-(isoquinolin-7-yl)-7a-methyltetrahydro-1H-inden-5(6H,7H,7aH)-ylidene]methyl}-N,N-dimethylcyclohex-3-enamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 6 steps
1.1: toluene-4-sulfonic acid / water; acetone / 2 h
2.1: 5% Pd/C / ethyl acetate / 12 h / Inert atmosphere
3.1: (bromomethyl)triphenyl phosphonium bromide / tetrahydrofuran / 3 h / 0 °C
3.2: 1 h / 0 °C
4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C
5.1: hydrogenchloride / ethanol / 3 h / 30 °C
6.1: sodium tris(acetoxy)borohydride / dichloromethane / 3 h / 30 °C
With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 5% Pd/C; (bromomethyl)triphenyl phosphonium bromide; sodium tris(acetoxy)borohydride; caesium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ml300143d
Guidance literature:
Multi-step reaction with 5 steps
1.1: 5% Pd/C / ethyl acetate / 12 h / Inert atmosphere
2.1: (bromomethyl)triphenyl phosphonium bromide / tetrahydrofuran / 3 h / 0 °C
2.2: 1 h / 0 °C
3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C
4.1: hydrogenchloride / ethanol / 3 h / 30 °C
5.1: sodium tris(acetoxy)borohydride / dichloromethane / 3 h / 30 °C
With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 5% Pd/C; (bromomethyl)triphenyl phosphonium bromide; sodium tris(acetoxy)borohydride; caesium carbonate; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ml300143d
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