Technology Process of N-(o-methoxyphenyl)dibenzazepine
There total 5 articles about N-(o-methoxyphenyl)dibenzazepine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 54.1 percent / anhydrous K2CO3, Cu / nitrobenzene / 14 h / Heating
2: 88.7 percent / diethyl maleate / Pd-C / 5 h / 210 °C
3: 21.9 percent / 85percent m-chloroperbenzoic acid, saturated aq. NaHCO3 / CH2Cl2; H2O / Ambient temperature
4: 45 mg / 30percent KOH / acetone / 0.5 h / Ambient temperature
With
potassium hydroxide; copper; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; Diethyl maleate;
palladium on activated charcoal;
In
dichloromethane; water; nitrobenzene; acetone;
DOI:10.1248/cpb.29.1221
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 54.1 percent / anhydrous K2CO3, Cu / nitrobenzene / 14 h / Heating
2: 88.7 percent / diethyl maleate / Pd-C / 5 h / 210 °C
3: 21.9 percent / 85percent m-chloroperbenzoic acid, saturated aq. NaHCO3 / CH2Cl2; H2O / Ambient temperature
4: 45 mg / 30percent KOH / acetone / 0.5 h / Ambient temperature
With
potassium hydroxide; copper; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; Diethyl maleate;
palladium on activated charcoal;
In
dichloromethane; water; nitrobenzene; acetone;
DOI:10.1248/cpb.29.1221
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 88.7 percent / diethyl maleate / Pd-C / 5 h / 210 °C
2: 21.9 percent / 85percent m-chloroperbenzoic acid, saturated aq. NaHCO3 / CH2Cl2; H2O / Ambient temperature
3: 45 mg / 30percent KOH / acetone / 0.5 h / Ambient temperature
With
potassium hydroxide; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; Diethyl maleate;
palladium on activated charcoal;
In
dichloromethane; water; acetone;
DOI:10.1248/cpb.29.1221
