(E)-alpha-Hydroxy-alpha-methylbenzeneacetic acid (1-(2-chlorophenyl)ethylidene)hydrazide

Base Information

• Chemical Name: (E)-alpha-Hydroxy-alpha-methylbenzeneacetic acid (1-(2-chlorophenyl)ethylidene)hydrazide
• CAS No.: 133687-85-1
• Molecular Formula: C₁₇H₁₇ClN₂O₂
• Molecular Weight: 316.787
• Nikkaji Number: J363.853G

Synonyms:BRN 4263308;(E)-alpha-Hydroxy-alpha-methylbenzeneacetic acid (1-(2-chlorophenyl)ethylidene)hydrazide;Benzeneacetic acid, alpha-hydroxy-alpha-methyl-, (1-(2-chlorophenyl)ethylidene)hydrazide, (E)-;Benzeneacetic acid, alpha-hydroxy-alpha-methyl-, (1-(2-chlorophenyl)ethylidene)hydrazide;133687-85-1;LS-28839;N'-(2-Chloro-alpha-methylbenzylidene)phenyl(methyl)hydroxyacetohydrazide

Chemical Property of (E)-alpha-Hydroxy-alpha-methylbenzeneacetic acid (1-(2-chlorophenyl)ethylidene)hydrazide

Chemical Property:

• XLogP3: 3.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 316.0978555
• Heavy Atom Count: 22
• Complexity: 421

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=NNC(=O)C(C)(C1=CC=CC=C1)O)C2=CC=CC=C2Cl
• Isomeric SMILES: C/C(=N\NC(=O)C(C)(C1=CC=CC=C1)O)/C2=CC=CC=C2Cl

Technology Process of (E)-alpha-Hydroxy-alpha-methylbenzeneacetic acid (1-(2-chlorophenyl)ethylidene)hydrazide

There total 1 articles about (E)-alpha-Hydroxy-alpha-methylbenzeneacetic acid (1-(2-chlorophenyl)ethylidene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1-(2-chlorophenyl)ethanone (2142-68-9) + 2-hydroxy-2-phenylpropionohydrazide (115248-48-1) → 2-Hydroxy-2-phenyl-propionic acid [1-(2-chloro-phenyl)-eth-(E)-ylidene]-hydrazide (133687-85-1)

Guidance literature:

In ethanol; for 4h; Heating;

DOI:10.1016/0223-5234(90)90198-C

upstream raw materials:

1-(2-chlorophenyl)ethanone

2-hydroxy-2-phenylpropionohydrazide

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