C₃₉H₃₈N₂O₆SSe

Base Information

Chemical Name:C₃₉H₃₈N₂O₆SSe
CAS No.:98664-93-8
Molecular Formula:C₃₉H₃₈N₂O₆SSe
Molecular Weight:741.767
Hs Code.:

C<sub>39</sub>H<sub>38</sub>N<sub>2</sub>O<sub>6</sub>SSe

Synonyms:

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Chemical Property of C₃₉H₃₈N₂O₆SSe

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Technology Process of C₃₉H₃₈N₂O₆SSe

There total 12 articles about C₃₉H₃₈N₂O₆SSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98665-02-2
(E)-2-(Formyl-methoxymethyl-amino)-3-[4-(3-oxo-butyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-acrylic acid ethyl ester

: 98664-93-8
C₃₉H₃₈N₂O₆SSe

Guidance literature:: Multi-step reaction with 6 steps

1: 50 percent / DBU / benzene / 6 h

2: 27 percent / DBU / benzene / 3.5 h

3: 2.) 50 percent NaH / 1.) THF, -80 deg C, 20 min, 2.) DMF, THF, from 0 deg C to RT, 1 h

4: 58 percent / 1 N HCl / dimethylsulfoxide; ethanol; H₂O / 2 h / Heating

5: 77 percent / Et₃N / CH₂Cl₂ / -20 - 20 °C

6: 1.) SiO₂ / 1.) CH₂Cl₂, -82 deg C, 15 min, 2.) CH₂Cl₂, RT, 1.5 h

With hydrogenchloride; silica gel; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In ethanol; dichloromethane; water; dimethyl sulfoxide; benzene;

Reference yield:

: 98665-03-3
(Z)-2-(Formyl-methoxymethyl-amino)-3-[4-(3-oxo-butyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-acrylic acid ethyl ester

: 98664-93-8
C₃₉H₃₈N₂O₆SSe

Guidance literature:: Multi-step reaction with 6 steps

1: 52 percent / DBU / benzene / 6 h

2: 27 percent / DBU / benzene / 3.5 h

3: 2.) 50 percent NaH / 1.) THF, -80 deg C, 20 min, 2.) DMF, THF, from 0 deg C to RT, 1 h

4: 58 percent / 1 N HCl / dimethylsulfoxide; ethanol; H₂O / 2 h / Heating

5: 77 percent / Et₃N / CH₂Cl₂ / -20 - 20 °C

6: 1.) SiO₂ / 1.) CH₂Cl₂, -82 deg C, 15 min, 2.) CH₂Cl₂, RT, 1.5 h

With hydrogenchloride; silica gel; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In ethanol; dichloromethane; water; dimethyl sulfoxide; benzene;

Reference yield:

: 98665-01-1
(Z)-2-(Formyl-methoxymethyl-amino)-3-[4-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-acrylic acid ethyl ester

: 98664-93-8
C₃₉H₃₈N₂O₆SSe

Guidance literature:: Multi-step reaction with 7 steps

1: 94 percent / acetone, p-Ts-OH / 14 h / Ambient temperature

2: 52 percent / DBU / benzene / 6 h

3: 27 percent / DBU / benzene / 3.5 h

4: 2.) 50 percent NaH / 1.) THF, -80 deg C, 20 min, 2.) DMF, THF, from 0 deg C to RT, 1 h

5: 58 percent / 1 N HCl / dimethylsulfoxide; ethanol; H₂O / 2 h / Heating

6: 77 percent / Et₃N / CH₂Cl₂ / -20 - 20 °C

7: 1.) SiO₂ / 1.) CH₂Cl₂, -82 deg C, 15 min, 2.) CH₂Cl₂, RT, 1.5 h

With hydrogenchloride; silica gel; sodium hydride; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; acetone; In ethanol; dichloromethane; water; dimethyl sulfoxide; benzene;