Benzaldehyde, 3-chloro-2-methyl-5-(3,7-dimethyl-2,6-octadienyl)-4,6-bis[[2-(trimethylsil yl)ethoxy]methoxy]-, (E)-

Base Information

• Chemical Name: Benzaldehyde, 3-chloro-2-methyl-5-(3,7-dimethyl-2,6-octadienyl)-4,6-bis[[2-(trimethylsil yl)ethoxy]methoxy]-, (E)-
• CAS No.: 105450-81-5
• Molecular Formula: C₃₀H₅₁ClO₅Si₂
• Molecular Weight: 583.356
• Mol file: 105450-81-5.mol

Synonyms:

Chemical Property of Benzaldehyde, 3-chloro-2-methyl-5-(3,7-dimethyl-2,6-octadienyl)-4,6-bis[[2-(trimethylsil yl)ethoxy]methoxy]-, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzaldehyde, 3-chloro-2-methyl-5-(3,7-dimethyl-2,6-octadienyl)-4,6-bis[[2-(trimethylsil yl)ethoxy]methoxy]-, (E)-

There total 6 articles about Benzaldehyde, 3-chloro-2-methyl-5-(3,7-dimethyl-2,6-octadienyl)-4,6-bis[[2-(trimethylsil yl)ethoxy]methoxy]-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[3-Chloro-5-((E)-3,7-dimethyl-octa-2,6-dienyl)-2-methyl-4,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-methanol (157826-53-4) → 3-Chloro-5-((E)-3,7-dimethyl-octa-2,6-dienyl)-2-methyl-4,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-benzaldehyde (105450-81-5)

Guidance literature:

With Pyr*CrO₃*HCl; In dichloromethane; Yield given;

DOI:10.1016/S0040-4039(00)84050-2

Reference yield:

trans-geranyl bromide (6138-90-5) → 3-Chloro-5-((E)-3,7-dimethyl-octa-2,6-dienyl)-2-methyl-4,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-benzaldehyde (105450-81-5)

Guidance literature:

Multi-step reaction with 3 steps

2: LiAlH₄ / diethyl ether

3: PyHCl*CrO₃ / CH₂Cl₂

With lithium aluminium tetrahydride; Pyr*CrO₃*HCl; In diethyl ether; dichloromethane;

DOI:10.1016/S0040-4039(00)84050-2

Reference yield:

2,4-dihydroxy-3-bromo-6-methyl-benzoic acid methyl ester (58106-55-1) → 3-Chloro-5-((E)-3,7-dimethyl-octa-2,6-dienyl)-2-methyl-4,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-benzaldehyde (105450-81-5)

Guidance literature:

Multi-step reaction with 5 steps

1: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

2: iPr₂NEt / CH₂Cl₂

4: LiAlH₄ / diethyl ether

5: PyHCl*CrO₃ / CH₂Cl₂

With lithium aluminium tetrahydride; sulfuryl dichloride; Pyr*CrO₃*HCl; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;

DOI:10.1016/S0040-4039(00)84050-2

upstream raw materials:

[3-Chloro-5-((E)-3,7-dimethyl-octa-2,6-dienyl)-2-methyl-4,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-methanol

trans-geranyl bromide

2,4-dihydroxy-3-bromo-6-methyl-benzoic acid methyl ester

3-Chloro-5-((E)-3,7-dimethyl-octa-2,6-dienyl)-2-methyl-4,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-benzoic acid methyl ester

Downstream raw materials:

3-chloro-5-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-4,6-dihydroxy-2-methylbenzaldehyde

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