S-(-)-5-benzyl-1-<(1'-aminomethyl-2'-hydroxyethoxy)methyl>uracil hydrochloride

Base Information

Chemical Name:S-(-)-5-benzyl-1-<(1'-aminomethyl-2'-hydroxyethoxy)methyl>uracil hydrochloride
CAS No.:130999-46-1
Molecular Formula:C₁₅H₁₉N₃O₄*ClH
Molecular Weight:341.794
Hs Code.:

Synonyms:

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Chemical Property of S-(-)-5-benzyl-1-<(1'-aminomethyl-2'-hydroxyethoxy)methyl>uracil hydrochloride

Chemical Property:

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Technology Process of S-(-)-5-benzyl-1-<(1'-aminomethyl-2'-hydroxyethoxy)methyl>uracil hydrochloride

There total 3 articles about S-(-)-5-benzyl-1-<(1'-aminomethyl-2'-hydroxyethoxy)methyl>uracil hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82857-71-4
2,4-dimethoxy-5-benzylpyrimidine

: 130999-46-1
S-(-)-5-benzyl-1-<(1'-aminomethyl-2'-hydroxyethoxy)methyl>uracil hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ (s) / CH₂Cl₂ / 48 h / Ambient temperature

2: 82 percent / 6 N HCl / methanol / 8 h / 40 °C

3: 1.) 98percent hydrazine; 2.) H₂, conc. HCl / 2.) 10percent Pd/C / 1.) methylene chloride, room temp., overnight; 2.) methanol, 3 atm.

With hydrogenchloride; hydrogen; potassium carbonate; hydrazine hydrate; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1002/jhet.5570250561

Reference yield:

: 119835-77-7
S-(-)-5-benzyl-1-<(1'-phtalimidomethyl-2'-benzyloxyethoxy)methyl>-2-oxo-4-methoxypyrimidine

: 130999-46-1
S-(-)-5-benzyl-1-<(1'-aminomethyl-2'-hydroxyethoxy)methyl>uracil hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 6 N HCl / methanol / 8 h / 40 °C

2: 1.) 98percent hydrazine; 2.) H₂, conc. HCl / 2.) 10percent Pd/C / 1.) methylene chloride, room temp., overnight; 2.) methanol, 3 atm.

With hydrogenchloride; hydrogen; hydrazine hydrate; palladium on activated charcoal; In methanol;
DOI:10.1002/jhet.5570250561

Reference yield:

: 119835-92-6
S-(-)-5-benzyl-1-<(1'-phtalimidomethyl-2'-benzyloxyethoxy)methyl>uracil

: 130999-46-1
S-(-)-5-benzyl-1-<(1'-aminomethyl-2'-hydroxyethoxy)methyl>uracil hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; hydrazine hydrate; palladium on activated charcoal; Yield given. Multistep reaction; 1.) methylene chloride, room temp., overnight; 2.) methanol, 3 atm.;
DOI:10.1002/jhet.5570250561