dichloro(tetraphemylporphyrinato)titanium(IV)

Base Information

Chemical Name:dichloro(tetraphemylporphyrinato)titanium(IV)
CAS No.:66350-83-2
Molecular Formula:C₄₄H₂₈Cl₂N₄Ti
Molecular Weight:731.519
Hs Code.:

Synonyms:

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Chemical Property of dichloro(tetraphemylporphyrinato)titanium(IV)

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Technology Process of dichloro(tetraphemylporphyrinato)titanium(IV)

There total 1 articles about dichloro(tetraphemylporphyrinato)titanium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58384-89-7
oxotitanium(IV) meso-tetraphenylporphinato

: 66350-83-2
dichloro(tetraphemylporphyrinato)titanium(IV)

Guidance literature:: With hydrogenchloride; In chloroform; passed HCl through soln.;

Reference yield: 34.0%

: 66350-83-2
dichloro(tetraphemylporphyrinato)titanium(IV)

: 4440-01-1
lithium phenylacetylide

: (meso-5,10,15,20-tetraphenylporphyrinato)Ti(1,2-η2-PhCCCCPh)

Guidance literature:: In tetrahydrofuran; toluene; to stirred soln. (TPP)TiCl2 in toluene/THF (10:1) at -25°C was added PhCCLi, soln. was kept at -25°C for 20 h; soln. was evapd. at room temp., residue was redissolved in toluene and filtered off, filtrate was layered with hexane and cooled to -25°C, ppt. was filtered, washed with hexane and dried in vacuo;
DOI:10.1021/ic9912575

Reference yield:

: 66350-83-2
dichloro(tetraphemylporphyrinato)titanium(IV)

: (meso-5,10,15,20-tetraphenylporphyrinato)Ti(pyridine)2

Guidance literature:: Multi-step reaction with 2 steps

1: toluene; tetrahydrofuran

2: benzene-d6

In tetrahydrofuran; benzene-d6; toluene;
DOI:10.1021/ic9912575