C₃₀H₂₉NO₆S

Base Information

Chemical Name:C₃₀H₂₉NO₆S
CAS No.:1268261-76-2
Molecular Formula:C₃₀H₂₉NO₆S
Molecular Weight:531.629
Hs Code.:

C<sub>30</sub>H<sub>29</sub>NO<sub>6</sub>S

Synonyms:

Suppliers and Price of C₃₀H₂₉NO₆S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₂₉NO₆S

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₃₀H₂₉NO₆S

There total 8 articles about C₃₀H₂₉NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1268261-74-0
C₃₀H₃₁NO₆S

: 1268261-76-2
C₃₀H₂₉NO₆S

: 1268261-82-0
C₃₀H₂₉NO₆S

: 1268261-75-1
C₃₀H₂₉NO₆S

Guidance literature:: With bis-[(trifluoroacetoxy)iodo]benzene; In acetonitrile; at -5 - 0 ℃; for 0.5h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201006367

Reference yield:

: 1268261-69-3
C₁₇H₁₆F₃NO₇S

: 1268261-76-2
C₃₀H₂₉NO₆S

: 1268261-82-0
C₃₀H₂₉NO₆S

: 1268261-75-1
C₃₀H₂₉NO₆S

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 2.5 h / 70 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 1.5 h / 25 °C

3: pyridine / dichloromethane / 12 h / 25 °C / Inert atmosphere

4: 20% palladium(II) hydroxide on carbon; hydrogen / ethyl acetate / 1.5 h / 25 °C

5: bis-[(trifluoroacetoxy)iodo]benzene / acetonitrile / 0.5 h / -5 - 0 °C / Inert atmosphere

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 20% palladium(II) hydroxide on carbon; palladium 10% on activated carbon; hydrogen; sodium carbonate; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; acetonitrile; 1: Suzuki-Miyaura reaction;
DOI:10.1002/anie.201006367

Reference yield:

: 1268261-71-7
C₃₁H₃₁NO₇

: 1268261-76-2
C₃₀H₂₉NO₆S

: 1268261-82-0
C₃₀H₂₉NO₆S

: 1268261-75-1
C₃₀H₂₉NO₆S

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 1.5 h / 25 °C

2: pyridine / dichloromethane / 12 h / 25 °C / Inert atmosphere

3: 20% palladium(II) hydroxide on carbon; hydrogen / ethyl acetate / 1.5 h / 25 °C

4: bis-[(trifluoroacetoxy)iodo]benzene / acetonitrile / 0.5 h / -5 - 0 °C / Inert atmosphere

With pyridine; 20% palladium(II) hydroxide on carbon; palladium 10% on activated carbon; hydrogen; bis-[(trifluoroacetoxy)iodo]benzene; In ethanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1002/anie.201006367