[(C₃H₇)3(C₆H₂)BH₂]2

Base Information

• Chemical Name: [(C₃H₇)3(C₆H₂)BH₂]2
• CAS No.: 158308-40-8
• Molecular Formula: C₃₀H₅₀B₂
• Molecular Weight: 432.349
• Mol file: 158308-40-8.mol

Synonyms:

Chemical Property of [(C₃H₇)3(C₆H₂)BH₂]2

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [(C₃H₇)3(C₆H₂)BH₂]2

There total 1 articles about [(C₃H₇)3(C₆H₂)BH₂]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

2[((C3H7)3C6H2)Li]*2O(C2H5)2 + monochloroborane-dimethyl sulfide → [(C3H7)3(C6H2)BH2]2 (158308-40-8)

Guidance literature:

In diethyl ether; reaction under N2: soln. of B-compd. in Et2O is treated with soln. of Li-organyl in the same solvent at 0°C, stirring for 12 h at room temp.; filtn., evapn. of all volatiles, recrystn. from n-hexane;

DOI:10.1039/DT9940002113

Reference yield: 73.0%

[(C3H7)3(C6H2)BH2]2 (158308-40-8) + thiophenol (108-98-5) → [((CH(CH3)2)3C6H2)B(SC6H5)2] (158174-99-3)

Guidance literature:

In hexane; reaction under N2: addn. of soln. of PhSH in n-hexane to a soln. of B-compd. in the same solvent at ambient temp., standing for 4 h; filtn. through Celite, concn. the volume and cooling to -20°C for crystn., recrystn. from pentane at 5°C;

DOI:10.1039/DT9940002113

Downstream raw materials:

[((CH(CH₃)2)3C₆H₂)B(SC₆H₅)2]