C₁₆HF₁₆N₃

Base Information

Chemical Name:C₁₆HF₁₆N₃
CAS No.:1130172-97-2
Molecular Formula:C₁₆HF₁₆N₃
Molecular Weight:539.178
Hs Code.:

C<sub>16</sub>HF<sub>16</sub>N<sub>3</sub>

Synonyms:

Suppliers and Price of C₁₆HF₁₆N₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆HF₁₆N₃

Chemical Property:

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Technology Process of C₁₆HF₁₆N₃

There total 1 articles about C₁₆HF₁₆N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 380-66-5
pentafluoroethyl-tetrafluoroethyliden-amine

: 771-60-8
2,3,4,5,6-pentafluoroaniline

: 1130172-97-2,1332479-85-2
C₁₆HF₁₆N₃

Guidance literature:: With triethylamine; at -5 - 20 ℃; Inert atmosphere;
DOI:10.1039/c1dt10524h

Reference yield: 90.6%

: 1130172-97-2,1332479-85-2
(N((CF₃)C(C₆F₅)N)2)H

: 75-05-8,26809-02-9
acetonitrile

: 20667-12-3
silver(l) oxide

: ([N((CF₃)C(C₆F₅)N)2]Ag(acetonitrile)2)n

Guidance literature:: In tetrahydrofuran; acetonitrile; under N2 and in flasks protected from light; a ligand (0.185 mmol) was added to a suspn. of Ag2O (0.14 mmol) in a mixt. of CH3CN and THF; the mixt. was refluxed for 16 h; the soln. was filtered over a bed of Celite and the solvent was removed from the filtrate under reduced pressure; the solid was dissolved in a min. amt. of CH2Cl2 and layered with hexanes; elem. anal.;
DOI:10.1039/c1dt10199d

Reference yield: 90.0%

: 1130172-97-2,1332479-85-2
(N((CF₃)C(C₆F₅)N)2)H

: 603-35-0
triphenylphosphine

: 20667-12-3
silver(l) oxide

: 1332831-35-2
[N((CF₃)C(C₆F₅)N)2]Ag(PPh₃)2

Guidance literature:: In diethyl ether; acetonitrile; (N2) ligand was added to suspn. Ag2O in MeCN, refluxed for 12 h, soln. was evapd. in vacuo, residue was dissolved in Et2O, PPh3 was added at room temp., stirred overnight; solvent was removed in vacuo, residue was recrystd. from n-hexane; elem.anal.;
DOI:10.1039/c1dt10524h