Technology Process of C14H18OS
There total 4 articles about C14H18OS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere
2: N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere
With
dmap; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo201027u
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonia; sodium / tetrahydrofuran / 8 h / Inert atmosphere
2: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere
3: N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere
With
dmap; ammonia; sodium; triethylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo201027u
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium amide; ferric nitrate / diethyl ether / 1 h / -78 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: ammonia; sodium / tetrahydrofuran / 8 h / Inert atmosphere
3.1: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere
4.1: N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere
With
dmap; lithium amide; ammonia; sodium; ferric nitrate; triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo201027u
