[η(5)-(2-diphenylphosphinoethyl)cyclopentadienyl](η(5)-cyclopentadienyl)dichlorozirconium

Base Information

Chemical Name:[η(5)-(2-diphenylphosphinoethyl)cyclopentadienyl](η(5)-cyclopentadienyl)dichlorozirconium
CAS No.:220313-47-3
Molecular Formula:C₂₄H₂₃Cl₂PZr
Molecular Weight:504.55
Hs Code.:

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Chemical Property of [η(5)-(2-diphenylphosphinoethyl)cyclopentadienyl](η(5)-cyclopentadienyl)dichlorozirconium

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Technology Process of [η(5)-(2-diphenylphosphinoethyl)cyclopentadienyl](η(5)-cyclopentadienyl)dichlorozirconium

There total 1 articles about [η(5)-(2-diphenylphosphinoethyl)cyclopentadienyl](η(5)-cyclopentadienyl)dichlorozirconium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.5%

: 220313-36-0
[η(5):η(1)-(2-diphenylphosphinoethyl)cyclopentadienyl]trichloro(tetrahydrofuran)zirconium(IV)

: 2726-34-3
cyclopentadienyltrimethyltin

: 220313-47-3
[η(5)-(2-diphenylphosphinoethyl)cyclopentadienyl](η(5)-cyclopentadienyl)dichlorozirconium

Guidance literature:: In toluene; sealed glass vessel (vac.); stirring (room temp., 3 h, 60°C, 2 h); evapn. (vac., 60°C), washing (heptane), drying (vac.), recrystn. (ether); elem. anal.;
DOI:10.1016/S0277-5387(98)00167-3

Reference yield: 95.0%

: 220313-47-3
[η(5)-(2-diphenylphosphinoethyl)cyclopentadienyl](η(5)-cyclopentadienyl)dichlorozirconium

: 7704-34-9
sulfur

: 885622-77-5
(η5-(2-diphenylphosphinothioethyl)cyclopentadienyl)(η5-cyclopentadienyl)dichlorozirconium

Guidance literature:: In toluene; using Schlenk techniques; soln. of S in toluene was added to soln. of Zrcomplex in toluene; mixt. stirred for 4 h; kept for 16 h; solvent removed; washed on filter (pentane); dried (high vac.); elem. anal.;
DOI:10.1007/s11172-005-0226-3