dimethylaminobenzaldehyde-zinc-bis(pentafluorothiophenolate)

Base Information

Chemical Name:dimethylaminobenzaldehyde-zinc-bis(pentafluorothiophenolate)
CAS No.:223446-86-4
Molecular Formula:C₂₁H₁₁F₁₀NOS₂Zn
Molecular Weight:612.83
Hs Code.:

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Chemical Property of dimethylaminobenzaldehyde-zinc-bis(pentafluorothiophenolate)

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Technology Process of dimethylaminobenzaldehyde-zinc-bis(pentafluorothiophenolate)

There total 2 articles about dimethylaminobenzaldehyde-zinc-bis(pentafluorothiophenolate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: bis(pentafluorophenylmercapto)zinc

: 579-72-6
2-(dimethylamino)benzaldehyde

: 223446-86-4
dimethylaminobenzaldehyde-zinc-bis(pentafluorothiophenolate)

Guidance literature:: In diethyl ether; acetone; N2-atmosphere; addn. of 2 equiv. aldehyde to Zn-compd. (pptn.); addn. of petroleum ether, collection (filtration), washing (petroleum ether), drying (vac.); elem. anal.;

Reference yield: 35.0%

: bis(pentafluorophenylmercapto)zinc

: 579-72-6
2-(dimethylamino)benzaldehyde

: 223446-86-4
dimethylaminobenzaldehyde-zinc-bis(pentafluorothiophenolate)

: 286387-23-3
dimethylaminobenzaldimine-zinc-bis(pentafluorothiophenolate)

Guidance literature:: In tetrahydrofuran; diethyl ether; soln. of 2-dimethylaminobenzaldehyde added dropwise with stirring to soln of Zn(SC6F5)2; pptd. (petroleum ether); filtered; dissolved (THF/CH2Cl2); soln. layered (petroleum ether); crystd. within 1 d; filtered off; washed (petroleum ether); dried in vacuo: elem. anal.;
DOI:10.1016/S0020-1693(99)00535-6