cis-PdCl2(2-phenyl-2-oxazoline)2

Base Information

• Chemical Name: cis-PdCl2(2-phenyl-2-oxazoline)2
• CAS No.: 1040261-24-2
• Molecular Formula: C₁₈H₁₈Cl₂N₂O₂Pd
• Molecular Weight: 471.679
• Mol file: 1040261-24-2.mol

Synonyms:

Chemical Property of cis-PdCl2(2-phenyl-2-oxazoline)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-PdCl2(2-phenyl-2-oxazoline)2

There total 4 articles about cis-PdCl2(2-phenyl-2-oxazoline)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2-phenyl-1,3-oxazoline (7127-19-7) + sodium tetrachloropalladate(II) → dichlorobis(2-phenyl-2-oxazoline)palladium(II) (287943-22-0,1040261-24-2)

Guidance literature:

In methanol; a soln. in abs. MeOH was stirred for 24 h at room temp.; ppt. was filtered, washed with MeOH, recrystd. from CHCl3-hexane; elem.anal.;

DOI:10.1016/S0022-328X(00)00133-9

Reference yield: 33.0%

2-phenyl-1,3-oxazoline (7127-19-7) + bis[(benzyldimethylamino)chloropalladium(II)] → dichlorobis(2-phenyl-2-oxazoline)palladium(II) (287943-22-0,1040261-24-2)

Guidance literature:

With CH₃COOH; In chloroform; a mixt. was stirred for 141 h at room temp.; ppt. was filtered, washed with AcOH and hexane, crystd. from CHCl3-hexane;

DOI:10.1016/S0022-328X(00)00133-9

Reference yield:

cis-PdCl2(2-phenyl-2-oxazoline)2 (287943-22-0,1040261-24-2) → dichlorobis(2-phenyl-2-oxazoline)palladium(II) (287943-22-0,1040261-24-2)

Guidance literature:

In chloroform-d1; keeping a soln. of palladium complex in CDCl3 at 294-313 K or heating at60°C for 8 h or at room temp. for 24 h; detected by NMR; Kinetics;

DOI:10.1039/b801951g

upstream raw materials:

2-phenyl-1,3-oxazoline

cis-PdCl2(2-phenyl-2-oxazoline)2

Downstream raw materials:

dichlorobis(2-phenyl-2-oxazoline)palladium(II)