dppfOSe

Base Information

• Chemical Name: dppfOSe
• CAS No.: 852547-08-1
• Molecular Formula: C₃₄H₂₈FeOP₂Se
• Molecular Weight: 649.35

Synonyms:

Chemical Property of dppfOSe

Chemical Property:

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Technology Process of dppfOSe

There total 1 articles about dppfOSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

selenium (7782-49-2) + (diphenylphosphinoyl)ferrocene → dppfOSe (852547-08-1)

Guidance literature:

In dichloromethane; under Ar; Fe complex dissolved in CH2Cl2 at room temp.; Se (1.1 equiv.) added; refluxed for 20 h with stirring; vol. reduced to half under vac.; MeOH added; cooled to 0°C for ca. 30 min; solvent decanted; crystals dried under vac.; elem. anal.;

DOI:10.1021/om050074p

upstream raw materials:

selenium

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