C₅₆H₇₂N₂O₂

Base Information

Chemical Name:C₅₆H₇₂N₂O₂
CAS No.:1364955-53-2
Molecular Formula:C₅₆H₇₂N₂O₂
Molecular Weight:805.2
Hs Code.:

C<sub>56</sub>H<sub>72</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₆H₇₂N₂O₂

Chemical Property:

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Technology Process of C₅₆H₇₂N₂O₂

There total 9 articles about C₅₆H₇₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 24544-04-5
2,6-diisopropylbenzenamine

: 1364955-52-1,1364955-65-6
C₃₂H₃₈O₄

: 1364955-53-2,1364955-67-8
C₅₆H₇₂N₂O₂

Guidance literature:: With toluene-4-sulfonic acid; In methanol; for 4h; Reflux;
DOI:10.1021/om2011694

Reference yield:

: 1646-54-4
1,4-dibromodurene

: 1364955-53-2,1364955-67-8
C₅₆H₇₂N₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 20 °C / Inert atmosphere; Cooling

1.2: 1 h / Cooling; Inert atmosphere

1.3: 120 h / 75 °C / Inert atmosphere

2.1: bromine; iron / dichloromethane / 3 h / 20 °C

3.1: tert.-butyl lithium / tetrahydrofuran; pentane / 20 °C / Inert atmosphere; Cooling

3.2: 20 °C / Cooling; Inert atmosphere

4.1: boron tribromide / dichloromethane / 1.5 h / Inert atmosphere

5.1: toluene-4-sulfonic acid / methanol / 4 h / Reflux

With bromine; tert.-butyl lithium; boron tribromide; iron; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; pentane; 1.1: Negishi coupling reaction / 1.2: Negishi coupling reaction / 1.3: Negishi coupling reaction;
DOI:10.1021/om2011694

Reference yield:

: 1364955-50-9,1364955-63-4
C₃₄H₄₂O₄

: 1364955-53-2,1364955-67-8
C₅₆H₇₂N₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1: boron tribromide / dichloromethane / 1.5 h / Inert atmosphere

2: toluene-4-sulfonic acid / methanol / 4 h / Reflux

With boron tribromide; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1021/om2011694