1-(((2E,6E)-8-((4-formylbenzoyl)oxy)-3,7-dimethylocta-2,6-dien-1-yl)oxy)-1,3,3-trihydroxy-1,3-dioxodiphosphoxane

Base Information

Chemical Name:1-(((2E,6E)-8-((4-formylbenzoyl)oxy)-3,7-dimethylocta-2,6-dien-1-yl)oxy)-1,3,3-trihydroxy-1,3-dioxodiphosphoxane
CAS No.:1376988-27-0
Molecular Formula:C₁₈H₂₄O₁₀P₂
Molecular Weight:462.33
Hs Code.:

Synonyms:

Suppliers and Price of 1-(((2E,6E)-8-((4-formylbenzoyl)oxy)-3,7-dimethylocta-2,6-dien-1-yl)oxy)-1,3,3-trihydroxy-1,3-dioxodiphosphoxane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(((2E,6E)-8-((4-formylbenzoyl)oxy)-3,7-dimethylocta-2,6-dien-1-yl)oxy)-1,3,3-trihydroxy-1,3-dioxodiphosphoxane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(((2E,6E)-8-((4-formylbenzoyl)oxy)-3,7-dimethylocta-2,6-dien-1-yl)oxy)-1,3,3-trihydroxy-1,3-dioxodiphosphoxane

There total 3 articles about 1-(((2E,6E)-8-((4-formylbenzoyl)oxy)-3,7-dimethylocta-2,6-dien-1-yl)oxy)-1,3,3-trihydroxy-1,3-dioxodiphosphoxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 1376988-42-9
(2E,6E)-8-hydroxy-2,6-dimethylocta-2,6-dien-1-yl 4-formylbenzoate

: 1376988-27-0
1-(((2E,6E)-8-((4-formylbenzoyl)oxy)-3,7-dimethylocta-2,6-dien-1-yl)oxy)-1,3,3-trihydroxy-1,3-dioxodiphosphoxane

Guidance literature:: With triethylammonium dihydrogen phosphate; trichloroacetonitrile; In acetonitrile; at 20 ℃; for 3.25h;
DOI:10.1021/ja211308s

Reference yield:

: 79577-53-0,110990-63-1,120732-61-8,120732-65-2,67858-93-9
2-(((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-yl)oxy)tetrahydro-2H-pyran

: 1376988-27-0
1-(((2E,6E)-8-((4-formylbenzoyl)oxy)-3,7-dimethylocta-2,6-dien-1-yl)oxy)-1,3,3-trihydroxy-1,3-dioxodiphosphoxane

Guidance literature:: Multi-step reaction with 4 steps

1: tert.-butylhydroperoxide; selenium(IV) oxide; salicylic acid

2: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

3: pyridinium p-toluenesulfonate / isopropyl alcohol / 4 h / 80 °C

4: triethylammonium dihydrogen phosphate; trichloroacetonitrile / acetonitrile / 3.25 h / 20 °C

With tert.-butylhydroperoxide; selenium(IV) oxide; triethylammonium dihydrogen phosphate; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; triethylamine; trichloroacetonitrile; salicylic acid; In dichloromethane; dimethyl sulfoxide; isopropyl alcohol; acetonitrile;
DOI:10.1021/ja211308s

Reference yield:

: 106-28-5
Farnesol

: 1376988-27-0
1-(((2E,6E)-8-((4-formylbenzoyl)oxy)-3,7-dimethylocta-2,6-dien-1-yl)oxy)-1,3,3-trihydroxy-1,3-dioxodiphosphoxane

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid

2: tert.-butylhydroperoxide; selenium(IV) oxide; salicylic acid

3: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

4: pyridinium p-toluenesulfonate / isopropyl alcohol / 4 h / 80 °C

5: triethylammonium dihydrogen phosphate; trichloroacetonitrile / acetonitrile / 3.25 h / 20 °C

With tert.-butylhydroperoxide; selenium(IV) oxide; triethylammonium dihydrogen phosphate; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; triethylamine; trichloroacetonitrile; salicylic acid; In dichloromethane; dimethyl sulfoxide; isopropyl alcohol; acetonitrile;
DOI:10.1021/ja211308s