Technology Process of 4-[2-((E)-2-Methoxy-vinyl)-phenyl]-butyric acid methyl ester
There total 4 articles about 4-[2-((E)-2-Methoxy-vinyl)-phenyl]-butyric acid methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: KOH / ethanol; H2O / 6 h / Heating
2: Li2CO3 / dimethylformamide / 20 h / Ambient temperature
3: 83 percent / pyridinium dichromate / dimethylformamide / 1.5 h / 0 - 20 °C
4: dimethylsulfoxide / 0.25 h / 15 °C
With
potassium hydroxide; dipyridinium dichromate; lithium carbonate;
In
ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm00362a002
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Li2CO3 / dimethylformamide / 20 h / Ambient temperature
2: 83 percent / pyridinium dichromate / dimethylformamide / 1.5 h / 0 - 20 °C
3: dimethylsulfoxide / 0.25 h / 15 °C
With
dipyridinium dichromate; lithium carbonate;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm00362a002
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 83 percent / pyridinium dichromate / dimethylformamide / 1.5 h / 0 - 20 °C
2: dimethylsulfoxide / 0.25 h / 15 °C
With
dipyridinium dichromate;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm00362a002
