[2-(2,4,6-trimethylphenyl)-4-methoxy-6-methyl pyrimidin-5-yl]dipropylamine

Base Information

Chemical Name:[2-(2,4,6-trimethylphenyl)-4-methoxy-6-methyl pyrimidin-5-yl]dipropylamine
CAS No.:360577-05-5
Molecular Formula:C₂₁H₃₁N₃O
Molecular Weight:341.497
Hs Code.:

Synonyms:

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Chemical Property of [2-(2,4,6-trimethylphenyl)-4-methoxy-6-methyl pyrimidin-5-yl]dipropylamine

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Technology Process of [2-(2,4,6-trimethylphenyl)-4-methoxy-6-methyl pyrimidin-5-yl]dipropylamine

There total 7 articles about [2-(2,4,6-trimethylphenyl)-4-methoxy-6-methyl pyrimidin-5-yl]dipropylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13162-26-0
2,4-dichloro-6-methyl-5-nitropyrimidine

: 360577-05-5
[2-(2,4,6-trimethylphenyl)-4-methoxy-6-methyl pyrimidin-5-yl]dipropylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 35 percent / methanol

2: [Pd(PPh₃)4]; NaHCO₃ / toluene / 70 °C

3: H₂ / Pd/C / atmospheric pressure

4: AcOH; NaBH(OAc)3 / 1,2-dichloro-ethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; acetic acid; palladium on activated charcoal; In methanol; 1,2-dichloro-ethane; toluene; 2: Suzuki coupling;
DOI:10.1016/S0960-894X(03)00483-9

Reference yield:

: 16632-21-6
6-methyl-5-nitropyrimidine-2,4-diol

: 360577-05-5
[2-(2,4,6-trimethylphenyl)-4-methoxy-6-methyl pyrimidin-5-yl]dipropylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / POCl₃; PhNEt₂ / Heating

2: 35 percent / methanol

3: [Pd(PPh₃)4]; NaHCO₃ / toluene / 70 °C

4: H₂ / Pd/C / atmospheric pressure

5: AcOH; NaBH(OAc)3 / 1,2-dichloro-ethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; acetic acid; N,N-diethylaniline; trichlorophosphate; palladium on activated charcoal; In methanol; 1,2-dichloro-ethane; toluene; 3: Suzuki coupling;
DOI:10.1016/S0960-894X(03)00483-9

Reference yield:

: 626-48-2
2,4-dihydroxy-6-methylpyrimidine

: 360577-05-5
[2-(2,4,6-trimethylphenyl)-4-methoxy-6-methyl pyrimidin-5-yl]dipropylamine

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / KNO₃; H₂SO₄

2: 60 percent / POCl₃; PhNEt₂ / Heating

3: 35 percent / methanol

4: [Pd(PPh₃)4]; NaHCO₃ / toluene / 70 °C

5: H₂ / Pd/C / atmospheric pressure

6: AcOH; NaBH(OAc)3 / 1,2-dichloro-ethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; hydrogen; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; acetic acid; potassium nitrate; N,N-diethylaniline; trichlorophosphate; palladium on activated charcoal; In methanol; 1,2-dichloro-ethane; toluene; 4: Suzuki coupling;
DOI:10.1016/S0960-894X(03)00483-9