Hydrazone de la 3-(2-benzyloxy-1-methylethyl)-2-<2-(p-methoxyphenoxy)ethyl>-2-methylcyclobutanone

Base Information

Chemical Name:Hydrazone de la 3-(2-benzyloxy-1-methylethyl)-2-<2-(p-methoxyphenoxy)ethyl>-2-methylcyclobutanone
CAS No.:125404-44-6
Molecular Formula:C₂₄H₃₂N₂O₃
Molecular Weight:396.53
Hs Code.:

Synonyms:

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Chemical Property of Hydrazone de la 3-(2-benzyloxy-1-methylethyl)-2-<2-(p-methoxyphenoxy)ethyl>-2-methylcyclobutanone

Chemical Property:

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Technology Process of Hydrazone de la 3-(2-benzyloxy-1-methylethyl)-2-<2-(p-methoxyphenoxy)ethyl>-2-methylcyclobutanone

There total 11 articles about Hydrazone de la 3-(2-benzyloxy-1-methylethyl)-2-<2-(p-methoxyphenoxy)ethyl>-2-methylcyclobutanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 125404-38-8
3-(2-Benzyloxy-1-methylethyl)-2-<2-(p-methoxyphenoxy)ethyl>-2-methylcyclobutanone

: 125404-44-6
Hydrazone de la 3-(2-benzyloxy-1-methylethyl)-2-<2-(p-methoxyphenoxy)ethyl>-2-methylcyclobutanone

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Heating;
DOI:10.1016/S0040-4020(01)87126-X

Reference yield:

: 517-23-7,594837-91-9,98634-97-0,313643-49-1
3-acetyl-2-oxo-4,5-dihydrofuran

: 125404-44-6
Hydrazone de la 3-(2-benzyloxy-1-methylethyl)-2-<2-(p-methoxyphenoxy)ethyl>-2-methylcyclobutanone

Guidance literature:: Multi-step reaction with 7 steps

1: 1) NaOMe / 1) MeOH, reflux, 1 h, 2) reflux, overnight

2: 82 percent / K₂CO₃ / H₂O / 12 h / 200 °C

3: SOCl₂, pyridine / diethyl ether / 1.5 h / Heating

4: H₂O / -15 °C

5: 1) COCl₂, 2) NEt₃ / 1) CH₂Cl₂, 0 deg C, 8 h, then rt, overnight, 2) CH₂Cl₂, 30-34 deg C to rt, 2 h

6: 1) ZnCl₂, 2) aq. Na₂CO₃ / 1) CH₂Cl₂, rt, overnight, 2) CH₂Cl₂, reflux

7: hydrazine hydrate / ethanol / 2 h / Heating

With pyridine; thionyl chloride; sodium methylate; sodium carbonate; potassium carbonate; hydrazine hydrate; triethylamine; zinc(II) chloride; In diethyl ether; ethanol; water;
DOI:10.1016/S0040-4020(01)87126-X

Reference yield:

: 4516-90-9
2-methyl-3-buten-1-ol

: 125404-44-6
Hydrazone de la 3-(2-benzyloxy-1-methylethyl)-2-<2-(p-methoxyphenoxy)ethyl>-2-methylcyclobutanone

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH / 1) DME, reflux, overnight, 2) reflux, 24 h

2: 1) ZnCl₂, 2) aq. Na₂CO₃ / 1) CH₂Cl₂, rt, overnight, 2) CH₂Cl₂, reflux

3: hydrazine hydrate / ethanol / 2 h / Heating

With sodium hydride; sodium carbonate; hydrazine hydrate; zinc(II) chloride; In ethanol;
DOI:10.1016/S0040-4020(01)87126-X