2-Propenoic acid, 2-methyl-, 7-(hexadecyloxy)-4-hydroxy-3,5,9-trioxa-4-phosphapentacosan-1-yl ester, P-oxide, sodium salt

Base Information

Chemical Name:2-Propenoic acid, 2-methyl-, 7-(hexadecyloxy)-4-hydroxy-3,5,9-trioxa-4-phosphapentacosan-1-yl ester, P-oxide, sodium salt
CAS No.:105501-11-9
Molecular Formula:C₄₁H₈₀O₈P*Na
Molecular Weight:755.045
Hs Code.:
Mol file:105501-11-9.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propenoic acid, 2-methyl-, 7-(hexadecyloxy)-4-hydroxy-3,5,9-trioxa-4-phosphapentacosan-1-yl ester, P-oxide, sodium salt

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Propenoic acid, 2-methyl-, 7-(hexadecyloxy)-4-hydroxy-3,5,9-trioxa-4-phosphapentacosan-1-yl ester, P-oxide, sodium salt

There total 3 articles about 2-Propenoic acid, 2-methyl-, 7-(hexadecyloxy)-4-hydroxy-3,5,9-trioxa-4-phosphapentacosan-1-yl ester, P-oxide, sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 868-77-9,141668-69-1,25736-86-1,82601-55-6,25249-16-5
2-methyl-2-propenoic acid 2-hydroxyethyl ester

: 74123-29-8
1,2-di-O-hexadecyl-rac-glycero-3-phosphoric acid dichloride

: 105501-11-9
sodium 2,3-bis(hexadecyloxy)propyl 3-methacryloyl-3-oxapropyl phosphate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 48h; Ambient temperature;
DOI:10.1021/ja00237a025

Reference yield:

: 6076-35-3
1,2-dihexadecylglycerol

: 105501-11-9
sodium 2,3-bis(hexadecyloxy)propyl 3-methacryloyl-3-oxapropyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / pyridine / CH₂Cl₂ / Heating

2: POCl₃, Et₃N / tetrahydrofuran / 1 h / -5 °C

3: 12 percent / Et₃N / tetrahydrofuran / 48 h / Ambient temperature

With pyridine; triethylamine; trichlorophosphate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00237a025

Reference yield:

: 96326-77-1
rac-1,2-di-O-hexadecyl-3-O-(3-carboxypropionyl)glycerol

: 105501-11-9
sodium 2,3-bis(hexadecyloxy)propyl 3-methacryloyl-3-oxapropyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃, Et₃N / tetrahydrofuran / 1 h / -5 °C

2: 12 percent / Et₃N / tetrahydrofuran / 48 h / Ambient temperature

With triethylamine; trichlorophosphate; In tetrahydrofuran;
DOI:10.1021/ja00237a025