(C₆H₅)2CNC(CS₂Pd(C₈H₁₂))COOC₂H₅

Base Information

Chemical Name:(C₆H₅)2CNC(CS₂Pd(C₈H₁₂))COOC₂H₅
CAS No.:582323-03-3
Molecular Formula:C₂₆H₂₇NO₂PdS₂
Molecular Weight:556.058
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>)2CNC(CS<sub>2</sub>Pd(C<sub>8</sub>H<sub>12</sub>))COOC<sub>2</sub>H<sub>5</sub>

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Suppliers and Price of (C₆H₅)2CNC(CS₂Pd(C₈H₁₂))COOC₂H₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₆H₅)2CNC(CS₂Pd(C₈H₁₂))COOC₂H₅

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Technology Process of (C₆H₅)2CNC(CS₂Pd(C₈H₁₂))COOC₂H₅

There total 1 articles about (C₆H₅)2CNC(CS₂Pd(C₈H₁₂))COOC₂H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 75-15-0,12122-00-8
carbon disulfide

: 12145-47-0
cis-dibromo-(cyclooctadiene)palladium(II)

: 69555-14-2
ethyl N-diphenylmethylene glycine

: 582323-03-3
(C₆H₅)2CNC(CS₂Pd(C₈H₁₂))COOC₂H₅

Guidance literature:: With n-BuLi; In tetrahydrofuran; N-compd. was dissolved in THF at -20 °C, 1 equiv. of CS2 was added, 2 equiv. of n-BuLi was added, 1 equiv. of metal-complex was added, within 12 h warmed to room temp.; solvent was removed in vac., residue was taken in CH2Cl2, soln. was filtered through Celite, concd. to half of its original vol., Et2O/petroleumether/pentane=1:4:2 mixt. was added, ppt. was washed with pentane, drie d in vac., elem. anal.;
DOI:10.1515/znb-2003-0410