Dimethyl meso-2,2'-dimethyl-4,4'-diphenyl-2,2'-azobutanoate

Base Information

Chemical Name:Dimethyl meso-2,2'-dimethyl-4,4'-diphenyl-2,2'-azobutanoate
CAS No.:132539-78-7
Molecular Formula:C₂₄H₃₀N₂O₄
Molecular Weight:410.513
Hs Code.:

Synonyms:

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Chemical Property of Dimethyl meso-2,2'-dimethyl-4,4'-diphenyl-2,2'-azobutanoate

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Technology Process of Dimethyl meso-2,2'-dimethyl-4,4'-diphenyl-2,2'-azobutanoate

There total 5 articles about Dimethyl meso-2,2'-dimethyl-4,4'-diphenyl-2,2'-azobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2550-26-7
4-Phenyl-2-butanone

: 132539-78-7,132539-79-8
Dimethyl meso-2,2'-dimethyl-4,4'-diphenyl-2,2'-azobutanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / 30percent aq. NH₄OH, NH₃-gas / methanol / 1) 0 deg C, 2 h 2) r.t., 4 d

2: 80 percent / conc. HCl / 48 h / Heating

3: 95 percent / SOCl₂ / 240 h / Ambient temperature

4: SO₂Cl₂ / pentane / 0.25 h / 0 °C

5: 1) NaOMe 2) t-BuOCl / 1) MeOH, 0 deg C, 0.5 h 2) MeOH, 0 deg C, 1 h

With hydrogenchloride; ammonium hydroxide; thionyl chloride; sulfuryl dichloride; tert-butylhypochlorite; sodium methylate; In methanol; pentane;
DOI:10.1021/jo00006a014

Reference yield:

: 96866-55-6
2-Amino-2-methyl-4-phenylbutanenitrile

: 132539-78-7,132539-79-8
Dimethyl meso-2,2'-dimethyl-4,4'-diphenyl-2,2'-azobutanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / conc. HCl / 48 h / Heating

2: 95 percent / SOCl₂ / 240 h / Ambient temperature

3: SO₂Cl₂ / pentane / 0.25 h / 0 °C

4: 1) NaOMe 2) t-BuOCl / 1) MeOH, 0 deg C, 0.5 h 2) MeOH, 0 deg C, 1 h

With hydrogenchloride; thionyl chloride; sulfuryl dichloride; tert-butylhypochlorite; sodium methylate; In pentane;
DOI:10.1021/jo00006a014

Reference yield:

: 132539-71-0
Methyl 2-amino-2-methyl-4-phenylbutanoate

: 132539-78-7,132539-79-8
Dimethyl meso-2,2'-dimethyl-4,4'-diphenyl-2,2'-azobutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: SO₂Cl₂ / pentane / 0.25 h / 0 °C

2: 1) NaOMe 2) t-BuOCl / 1) MeOH, 0 deg C, 0.5 h 2) MeOH, 0 deg C, 1 h

With sulfuryl dichloride; tert-butylhypochlorite; sodium methylate; In pentane;
DOI:10.1021/jo00006a014