2,3,3-trimethyl-2-phenyltetrahydrofuran

Base Information

Chemical Name:2,3,3-trimethyl-2-phenyltetrahydrofuran
CAS No.:1408286-12-3
Molecular Formula:C₁₃H₁₈O
Molecular Weight:190.285
Hs Code.:

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Chemical Property of 2,3,3-trimethyl-2-phenyltetrahydrofuran

Chemical Property:

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Technology Process of 2,3,3-trimethyl-2-phenyltetrahydrofuran

There total 3 articles about 2,3,3-trimethyl-2-phenyltetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1408286-11-2
3,3-dimethyl-4-phenylpent-4-en-1-ol

: 1408286-12-3
2,3,3-trimethyl-2-phenyltetrahydrofuran

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; for 3h; Inert atmosphere;
DOI:10.1021/ja309635w

Reference yield:

: 1408286-35-0
3,3-dimethyl-4-phenylpent-4-enoic acid

: 1408286-12-3
2,3,3-trimethyl-2-phenyltetrahydrofuran

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; lithium aluminium tetrahydride / tetrahydrofuran; water / 0.17 h / 0 - 25 °C / Inert atmosphere

2: trifluorormethanesulfonic acid / dichloromethane / 3 h / Inert atmosphere

With lithium aluminium tetrahydride; trifluorormethanesulfonic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja309635w

Reference yield:

: 39576-24-4
2,2-dimethyl-1-phenyl-4-pentene

: 1408286-12-3
2,3,3-trimethyl-2-phenyltetrahydrofuran

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; acetic acid; potassium permanganate / dichloromethane / Cooling with ice

1.2: Inert atmosphere

2.1: sodium hydroxide; lithium aluminium tetrahydride / tetrahydrofuran; water / 0.17 h / 0 - 25 °C / Inert atmosphere

3.1: trifluorormethanesulfonic acid / dichloromethane / 3 h / Inert atmosphere

With potassium permanganate; lithium aluminium tetrahydride; trifluorormethanesulfonic acid; sulfuric acid; acetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja309635w