Technology Process of 4,5-diethyl-4,5-dimethyl-2-phenyl-1,3-oxathiolane
There total 5 articles about 4,5-diethyl-4,5-dimethyl-2-phenyl-1,3-oxathiolane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / benzene; diethyl ether / 2 - 20 °C
2: 62 percent / sodium in ammonia, ammonium chloride / diethyl ether / 0.33 h
3: toluene-p-sulphonic acid / benzene / Heating
With
ammonium hydroxide; ammonium chloride; sodium; toluene-4-sulfonic acid;
In
diethyl ether; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) NaH / 1.) THF, reflux, 30 m, 2.) THF, 25 deg C, reflux, 3 h
2: 71 percent / MgBr2 / diethyl ether / Heating
3: 62 percent / sodium in ammonia, ammonium chloride / diethyl ether / 0.33 h
4: toluene-p-sulphonic acid / benzene / Heating
With
ammonium hydroxide; ammonium chloride; sodium; sodium hydride; toluene-4-sulfonic acid; magnesium bromide;
In
diethyl ether; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 71 percent / MgBr2 / diethyl ether / Heating
2: 62 percent / sodium in ammonia, ammonium chloride / diethyl ether / 0.33 h
3: toluene-p-sulphonic acid / benzene / Heating
With
ammonium hydroxide; ammonium chloride; sodium; toluene-4-sulfonic acid; magnesium bromide;
In
diethyl ether; benzene;