C₃₇H₅₃BIN₃O₁₀

Base Information

Chemical Name:C₃₇H₅₃BIN₃O₁₀
CAS No.:1415464-76-4
Molecular Formula:C₃₇H₅₃BIN₃O₁₀
Molecular Weight:837.557
Hs Code.:

C<sub>37</sub>H<sub>53</sub>BIN<sub>3</sub>O<sub>10</sub>

Synonyms:

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Chemical Property of C₃₇H₅₃BIN₃O₁₀

Chemical Property:

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Technology Process of C₃₇H₅₃BIN₃O₁₀

There total 7 articles about C₃₇H₅₃BIN₃O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71460-02-1,173306-82-6
methyl (2S)-2-(tert-butoxycarbonylamino)pent-4-ynoate

: 1415464-76-4
C₃₇H₅₃BIN₃O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / 15 °C

1.2: 15 °C

2.1: hydrogen / palladium on activated charcoal / methanol / 3 h / 15 °C

3.1: iodine; silver sulfate / methanol

4.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 0.75 h / 80 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 15 °C

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; acetonitrile / 15 °C

With hydrogen; iodine; potassium acetate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; palladium on activated charcoal; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1415464-72-0
C₁₈H₂₃NO₅

: 1415464-76-4
C₃₇H₅₃BIN₃O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen / palladium on activated charcoal / methanol / 3 h / 15 °C

2: iodine; silver sulfate / methanol

3: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 0.75 h / 80 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 15 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; acetonitrile / 15 °C

With hydrogen; iodine; potassium acetate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium on activated charcoal; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 696-62-8
para-iodoanisole

: 1415464-76-4
C₃₇H₅₃BIN₃O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / 15 °C

1.2: 15 °C

2.1: hydrogen / palladium on activated charcoal / methanol / 3 h / 15 °C

3.1: iodine; silver sulfate / methanol

4.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 0.75 h / 80 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 15 °C

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; acetonitrile / 15 °C

With hydrogen; iodine; potassium acetate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; palladium on activated charcoal; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;