mer-tris(phenyldibenzophosphole)tricarbonyltungsten⁽⁰⁾*methanol

Base Information

Chemical Name:mer-tris(phenyldibenzophosphole)tricarbonyltungsten⁽⁰⁾*methanol
CAS No.:114860-50-3
Molecular Formula:CH₄O*C₅₇H₃₉O₃P₃W
Molecular Weight:1080.75
Hs Code.:

mer-tris(phenyldibenzophosphole)tricarbonyltungsten<sup>(0)</sup>*methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mer-tris(phenyldibenzophosphole)tricarbonyltungsten⁽⁰⁾*methanol

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Technology Process of mer-tris(phenyldibenzophosphole)tricarbonyltungsten⁽⁰⁾*methanol

There total 1 articles about mer-tris(phenyldibenzophosphole)tricarbonyltungsten⁽⁰⁾*methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 14040-11-0
tungsten hexacarbonyl

: 1088-00-2
9-phenyl-9-phosphafluorene

: 114860-50-3
mer-tris(phenyldibenzophosphole)tricarbonyltungsten⁽⁰⁾*methanol

: 114860-49-0
cis-bis(phenyldibenzophosphole)tetracarbonyltungsten⁽⁰⁾

Guidance literature:: With catalyst:(CH₃)3NO*2H₂O; In diethylene glycol dimethyl ether; Refluxing a mixture of W(CO)6 and DBP in diglyme for 14 days (N2), after 24 h of reflux Me3NO*2H2O is added.; Evaporation on a rotary evaporator with heat, fractional crystn. with CH2Cl2/MeOH yields tricarbonyl complex, elem. anal.;
DOI:10.1021/om00098a006