((NC₅H₄)2NC₅H₂C₆H₄CCC₆H₄)2C₂B₁₀H₁₀

Base Information

Chemical Name:((NC₅H₄)2NC₅H₂C₆H₄CCC₆H₄)2C₂B₁₀H₁₀
CAS No.:1274612-67-7
Molecular Formula:C₆₀H₄₆B₁₀N₆
Molecular Weight:959.175
Hs Code.:

((NC<sub>5</sub>H<sub>4</sub>)2NC<sub>5</sub>H<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CCC<sub>6</sub>H<sub>4</sub>)2C<sub>2</sub>B<sub>10</sub>H<sub>10</sub>

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Chemical Property of ((NC₅H₄)2NC₅H₂C₆H₄CCC₆H₄)2C₂B₁₀H₁₀

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Technology Process of ((NC₅H₄)2NC₅H₂C₆H₄CCC₆H₄)2C₂B₁₀H₁₀

There total 1 articles about ((NC₅H₄)2NC₅H₂C₆H₄CCC₆H₄)2C₂B₁₀H₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 71482-44-5
1,2-bis(4-iodophenyl)-ortho-carborane

: 149817-61-8
4'-(4-ethynylphenyl)-2,2':6',2-terpyridine

: 1274612-67-7
((NC₅H₄)2NC₅H₂C₆H₄CCC₆H₄)2C₂B₁₀H₁₀

Guidance literature:: With Pd(PPh₃)4; CuI; triethylamine; In tetrahydrofuran; (Ar) 1,3-bis(4-iodophenyl)-o-carborane, 4'-(4-ethynylphenyl)-2,2':6',2''-terpyridine, Pd(PPh3)4 and CuI were dissolved in THF, Et3N was added, refluxed for 24 h; CHCl3 was added, washed with aq. NH3 soln., water and brine, prg. layer was dried over MgSO4, filtered and evapd., chromy. on alumina (CHCl3-Et3N 90/10);
DOI:10.1039/c1dt90011k

Reference yield: 83.0%

: ammonium hexafluorophosphate

: 1274612-67-7
((NC₅H₄)2NC₅H₂C₆H₄CCC₆H₄)2C₂B₁₀H₁₀

: 5970-45-6
zinc(II) acetate dihydrate

: Zn⁽²⁺⁾*((NC₅H₄)2NC₅H₂C₆H₄CCC₆H₄)2C₂B₁₀H₁₀*2PF₆^(1-)=(Zn(((NC₅H₄)2NC₅H₂C₆H₄CCC₆H₄)2C₂B₁₀H₁₀))(PF₆)2

Guidance literature:: In methanol; chloroform; (Ar) to soln. ligand in CHCl3 soln. Zn(OAc)2*2H2O in MeOH was added, stirred for 1 h at room temp., NH4PF6 was added; soln. was poured into ether, ppt. was collected;
DOI:10.1039/c1dt90011k