Technology Process of C24H32N4O5
There total 6 articles about C24H32N4O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H34N4O5;
With
sodium hydroxide;
In
acetonitrile;
at 20 ℃;
for 3h;
With
hydrogenchloride;
In
water; acetonitrile;
DOI:10.1002/chir.22160
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium cyanoborohydride / ethanol / 0.5 h
2: sodium cyanoborohydride / ethanol / 0.5 h
3: thionyl chloride / dichloromethane / 5 h / -10 - 25 °C
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h
5: sodium hydroxide / acetonitrile / 3 h / 20 °C
With
thionyl chloride; sodium cyanoborohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
ethanol; dichloromethane; acetonitrile;
DOI:10.1002/chir.22160
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium cyanoborohydride / ethanol / 0.5 h
2: thionyl chloride / dichloromethane / 5 h / -10 - 25 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h
4: sodium hydroxide / acetonitrile / 3 h / 20 °C
With
thionyl chloride; sodium cyanoborohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
ethanol; dichloromethane; acetonitrile;
DOI:10.1002/chir.22160