Pd(CS₂)(P(C₆H₅)2CH₂CH₂)2

Base Information

Chemical Name:Pd(CS₂)(P(C₆H₅)2CH₂CH₂)2
CAS No.:81191-63-1
Molecular Formula:C₂₉H₂₈P₂PdS₂
Molecular Weight:609.041
Hs Code.:

Pd(CS<sub>2</sub>)(P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>CH<sub>2</sub>)2

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Chemical Property of Pd(CS₂)(P(C₆H₅)2CH₂CH₂)2

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Technology Process of Pd(CS₂)(P(C₆H₅)2CH₂CH₂)2

There total 1 articles about Pd(CS₂)(P(C₆H₅)2CH₂CH₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 52522-40-4
tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex

: 7688-25-7
1,4-di(diphenylphosphino)-butane

: 81191-63-1
Pd(CS₂)(P(C₆H₅)2CH₂CH₂)2

Guidance literature:: With carbon disulfide; In diethyl ether; byproducts: CHCl3, dibenzylideneacetone; to a suspension of Pd-complex in Et2O were added ligand and CS2, stirred at room temp.; filtered, washed with Et2O, dried in a N2 stream and in vac.; elem. anal.;

Reference yield:

: 10544-50-0
sulfur

: 81191-63-1
(1,4-bis(diphenylphosphino)butane)2(η2-CS2)palladium

: 7688-25-7
1,4-di(diphenylphosphino)-butane

: 86802-35-9
((C₆H₅)2P(CH₂)4P(C₆H₅)2)Pd(S₂CS)

Guidance literature:: In carbon disulfide; chloroform; benzene; addn. of S8 to a soln. of the Pd-compd. in benzene and CS2, stirring for 72 h, evapn. of the soln. to dryness and the residue is extd. with CHCl3, addn. of the phosphine whilst the stirring at room temp. is continued for 3 h; the soln. is evapd. partially, crystn. on addn. of Et2O, sepn. of the mixt. of Pd-compd. and phosphine sulfide by chromy. (Florisil columns, benzene/CH2Cl2); elem. anal.;