nonanedioic acid phenylamide (2-tritylsulfanyl-ethyl)-amide

Base Information

Chemical Name:nonanedioic acid phenylamide (2-tritylsulfanyl-ethyl)-amide
CAS No.:852619-60-4
Molecular Formula:C₃₆H₄₀N₂O₂S
Molecular Weight:564.792
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of nonanedioic acid phenylamide (2-tritylsulfanyl-ethyl)-amide

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Technology Process of nonanedioic acid phenylamide (2-tritylsulfanyl-ethyl)-amide

There total 4 articles about nonanedioic acid phenylamide (2-tritylsulfanyl-ethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1095-85-8
2-amino tritylthio ethane

: 73148-09-1
8-phenylcarbamoyl-octanoic acid

: 852619-60-4
nonanedioic acid phenylamide (2-tritylsulfanyl-ethyl)-amide

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2005.02.075

Reference yield:

: 852619-53-5
8-phenylcarbamoyl-octanoic acid methyl ester

: 852619-60-4
nonanedioic acid phenylamide (2-tritylsulfanyl-ethyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. LiOH / ethanol / 3 h / 20 °C

2: EDC; HOBt; DIEA / CH₂Cl₂ / 12 h / 20 °C

With lithium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2005.02.075

Reference yield:

: 2104-19-0
azelaic monomethyl ester

: 852619-60-4
nonanedioic acid phenylamide (2-tritylsulfanyl-ethyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: EDCI; HOBt; DIEA / 9 h / 20 °C

2: aq. LiOH / ethanol / 3 h / 20 °C

3: EDC; HOBt; DIEA / CH₂Cl₂ / 12 h / 20 °C

With lithium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2005.02.075