1,2-bis[5-(3,4,5-tri(2-[2-(2-(2-[2-(2-methoxyethoxy)ethoxy]ethoxy)ethoxy)ethoxy]ethoxy)phenyl)2-methylthiophen-3-yl]perfluorocyclopentene

Base Information

Chemical Name:1,2-bis[5-(3,4,5-tri(2-[2-(2-(2-[2-(2-methoxyethoxy)ethoxy]ethoxy)ethoxy)ethoxy]ethoxy)phenyl)2-methylthiophen-3-yl]perfluorocyclopentene
CAS No.:1135950-08-1
Molecular Formula:C₁₀₅H₁₇₄F₆O₄₂S₂
Molecular Weight:2286.63
Hs Code.:

1,2-bis[5-(3,4,5-tri(2-[2-(2-(2-[2-(2-methoxyethoxy)ethoxy]ethoxy)ethoxy)ethoxy]ethoxy)phenyl)2-methylthiophen-3-yl]perfluorocyclopentene

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Chemical Property of 1,2-bis[5-(3,4,5-tri(2-[2-(2-(2-[2-(2-methoxyethoxy)ethoxy]ethoxy)ethoxy)ethoxy]ethoxy)phenyl)2-methylthiophen-3-yl]perfluorocyclopentene

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Technology Process of 1,2-bis[5-(3,4,5-tri(2-[2-(2-(2-[2-(2-methoxyethoxy)ethoxy]ethoxy)ethoxy)ethoxy]ethoxy)phenyl)2-methylthiophen-3-yl]perfluorocyclopentene

There total 2 articles about 1,2-bis[5-(3,4,5-tri(2-[2-(2-(2-[2-(2-methoxyethoxy)ethoxy]ethoxy)ethoxy)ethoxy]ethoxy)phenyl)2-methylthiophen-3-yl]perfluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.1%

: 1135950-12-7
5-bromo-1,2,3-tris-(2-[2-(2-(2-[2-(2-methoxyethoxy)ethoxy]ethoxy)ethoxy)ethoxy]ethoxy)benzene

: 3-(3,3,4,4,5,5-hexafluoro-2-(5-iodo-2-methylthiophen-3-yl)cyclopent-1-enyl)-5-iodo-2-methylthiophene

: 1135950-08-1
1,2-bis[5-(3,4,5-tri(2-[2-(2-(2-[2-(2-methoxyethoxy)ethoxy]ethoxy)ethoxy)ethoxy]ethoxy)phenyl)2-methylthiophen-3-yl]perfluorocyclopentene

Guidance literature:: 3-(3,3,4,4,5,5-hexafluoro-2-(5-iodo-2-methylthiophen-3-yl)cyclopent-1-enyl)-5-iodo-2-methylthiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

With boric acid tributyl ester; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

5-bromo-1,2,3-tris-(2-[2-(2-(2-[2-(2-methoxyethoxy)ethoxy]ethoxy)ethoxy)ethoxy]ethoxy)benzene; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; hexane; water; for 16h; Reflux; Inert atmosphere;
DOI:10.1002/asia.200800340