Technology Process of C23H24FN3O5
There total 6 articles about C23H24FN3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ethanol / Heating
1.2: 20 °C
2.1: O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate; triethylamine / N,N-dimethyl-formamide
3.1: 1,2-dichloro-ethane / Heating
With
triethylamine; O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate;
In
ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
3.2: |Dieckmann Condensation;
DOI:10.1016/j.bmcl.2014.05.011
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,2-dichloro-ethane / Heating
2: sodium ethanolate / ethanol
With
sodium ethanolate;
In
ethanol; 1,2-dichloro-ethane;
1: |Dieckmann Condensation / 2: |Dieckmann Condensation;
DOI:10.1016/j.bmcl.2014.05.011
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium cyanoborohydride / 20 °C
2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide
3: 1,2-dichloro-ethane / Heating
4: sodium ethanolate / ethanol
With
sodium ethanolate; sodium cyanoborohydride; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
3: |Dieckmann Condensation / 4: |Dieckmann Condensation;
DOI:10.1016/j.bmcl.2014.05.011