C₅₉H₆₆AuNO

Base Information

Chemical Name:C₅₉H₆₆AuNO
CAS No.:1447801-26-4
Molecular Formula:C₅₉H₆₆AuNO
Molecular Weight:1002.15
Hs Code.:

Synonyms:

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Chemical Property of C₅₉H₆₆AuNO

Chemical Property:

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Technology Process of C₅₉H₆₆AuNO

There total 7 articles about C₅₉H₆₆AuNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-(3,5-di-tert-butylphenyl)-1-(9,9-dihexyl-9H-fluoren-2-yl)prop-2-en-1-one

: 1447801-26-4
C₅₉H₆₆AuNO

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium acetate; acetic acid / methanol / Reflux

2.1: ethanol / 48 h / Reflux

2.2: 2 h / Reflux

3.1: acetonitrile / 48 h / Reflux

4.1: triethylamine; copper(l) iodide / dichloromethane / 3 h / Inert atmosphere

With copper(l) iodide; ammonium acetate; acetic acid; triethylamine; In methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1002/anie.201301149

Reference yield:

: 86-73-7
9H-fluorene

: 1447801-26-4
C₅₉H₆₆AuNO

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium tert-butylate / tetrahydrofuran / Inert atmosphere; Reflux

2.1: carbon disulfide; aluminum (III) chloride / 3 h / Inert atmosphere; Reflux

3.1: sodium hydroxide / methanol / 0.17 h

3.2: 60 °C

4.1: ammonium acetate; acetic acid / methanol / Reflux

5.1: ethanol / 48 h / Reflux

5.2: 2 h / Reflux

6.1: acetonitrile / 48 h / Reflux

7.1: triethylamine; copper(l) iodide / dichloromethane / 3 h / Inert atmosphere

With carbon disulfide; aluminum (III) chloride; copper(l) iodide; potassium tert-butylate; ammonium acetate; acetic acid; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1002/anie.201301149

Reference yield:

: 610788-00-6
9,9-di-n-hexyl-2-acetylfluorene

: 1447801-26-4
C₅₉H₆₆AuNO

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / methanol / 0.17 h

1.2: 60 °C

2.1: ammonium acetate; acetic acid / methanol / Reflux

3.1: ethanol / 48 h / Reflux

3.2: 2 h / Reflux

4.1: acetonitrile / 48 h / Reflux

5.1: triethylamine; copper(l) iodide / dichloromethane / 3 h / Inert atmosphere

With copper(l) iodide; ammonium acetate; acetic acid; triethylamine; sodium hydroxide; In methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1002/anie.201301149