[Ru(η6-4-phenyl-2-butanol)(1,3,5-triaza-7-phosphatricyclo[3.3.1.1]decane)Cl(triphenylphosphine)]BF4

Base Information

Chemical Name:[Ru(η6-4-phenyl-2-butanol)(1,3,5-triaza-7-phosphatricyclo[3.3.1.1]decane)Cl(triphenylphosphine)]BF4
CAS No.:1211431-72-9
Molecular Formula:BF₄*C₃₄H₄₁ClN₃OP₂Ru
Molecular Weight:792.994
Hs Code.:

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Chemical Property of [Ru(η6-4-phenyl-2-butanol)(1,3,5-triaza-7-phosphatricyclo[3.3.1.1]decane)Cl(triphenylphosphine)]BF4

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Technology Process of [Ru(η6-4-phenyl-2-butanol)(1,3,5-triaza-7-phosphatricyclo[3.3.1.1]decane)Cl(triphenylphosphine)]BF4

There total 1 articles about [Ru(η6-4-phenyl-2-butanol)(1,3,5-triaza-7-phosphatricyclo[3.3.1.1]decane)Cl(triphenylphosphine)]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 13826-83-0
ammonium tetrafluroborate

: 876728-15-3
[Ru(η6-4-phenyl-2-butanol)(1,3,5-triaza-7-phosphatricyclo[3.3.1.1]decane)Cl2]

: 603-35-0
triphenylphosphine

: 1211431-72-9,1213241-61-2
[Ru(η6-4-phenyl-2-butanol)(1,3,5-triaza-7-phosphatricyclo[3.3.1.1]decane)Cl(triphenylphosphine)]BF4

Guidance literature:: In methanol; using standard Schlenk techniques; NH4BF4 and Ru complex refluxed in MeCN for 1 h; soln. filtered; solvent removed at reduced pressure; extd. with MeOH; pptd. with Et2O; ppt. and ligand (excess) in MeOH stirred at room temp. for 5 h; solvent vol. reduced; pptd. with hexane; ppt. washed with hexane and Et2O;
DOI:10.1021/ic9020433