ethyl[1-benzoyl-4-cyano-3-(methylthio)-1H-pyrazol-5-yl]imidoformate

Base Information

Chemical Name:ethyl[1-benzoyl-4-cyano-3-(methylthio)-1H-pyrazol-5-yl]imidoformate
CAS No.:1382684-40-3
Molecular Formula:C₁₅H₁₄N₄O₂S
Molecular Weight:314.368
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl[1-benzoyl-4-cyano-3-(methylthio)-1H-pyrazol-5-yl]imidoformate

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Technology Process of ethyl[1-benzoyl-4-cyano-3-(methylthio)-1H-pyrazol-5-yl]imidoformate

There total 1 articles about ethyl[1-benzoyl-4-cyano-3-(methylthio)-1H-pyrazol-5-yl]imidoformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 5-amino-1-benzoyl-3-(methylthio)-1H-pyrazole-4-carbonitrile

: 122-51-0
orthoformic acid triethyl ester

: 1382684-40-3
ethyl[1-benzoyl-4-cyano-3-(methylthio)-1H-pyrazol-5-yl]imidoformate

Guidance literature:: With acetic anhydride; for 6h; Reflux;
DOI:10.1080/00397911.2011.566462

Reference yield:

: 1382684-40-3
ethyl[1-benzoyl-4-cyano-3-(methylthio)-1H-pyrazol-5-yl]imidoformate

: 1382684-38-9
N-[1-benzoyl-4-cyano-3-(methylthio)-1H-pyrazol-5-yl]acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine

2: N,N-dimethyl-formamide / 3.5 h / 20 °C / Reflux

With hydrazine; In N,N-dimethyl-formamide;
DOI:10.1080/00397911.2011.566462

Reference yield:

: 1382684-40-3
ethyl[1-benzoyl-4-cyano-3-(methylthio)-1H-pyrazol-5-yl]imidoformate

: 1382684-30-1
1-benzoyl-3-(methylthio)-5-(1H-pyrrol-1-yl)-1H-pyrazole-4-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine

2: acetic acid / 1 h / Reflux

With acetic acid; hydrazine;
DOI:10.1080/00397911.2011.566462